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Appendix D


                       Experimental Methods for

                                 Elastomer Pipes







             The purpose  of  this  appendix  is to present  some of  the techniques,  developed  over the
             past  30 years  in  the  author’s laboratories,  for  manufacturing  elastomer  pipes,  shells  or
             cylinders, as well as for determining some of  their key physical properties. It is recalled
             that  experimentation  with elastomer  flexible structures translates into low-pressure test-
             rigs,  and  hence  easier  experiments  than  with  stiffer bodies,  e.g. made  of  metal.  In  the
             case of  pipes, the home-made  ones are far  superior to those commercially  available, as
             explained for example in Section 3.5.6.


             D.l  MATERIALS, EQUIPMENT AND PROCEDURES

             In  most  cases,  the  material  used  for  making  the  flexible bodies  is  a room-temperature
             vulcanizing  (RTV) silicone  rubber  (e.g. ‘Silastic E RTV’ made by  Dow  Corning).  It  is
             supplied  in  a two-component  kit,  and  the  two  fluids, one  of  which  is  the  catalyst,  are
             mixed  in  the  prescribed  ratio  (typically  1O:l) just  before  manufacture.  The  mixture  is
             poured  into  a mould,  cured,  and  then  extracted,  as  described  in  what  follows.  Another
             essential item is a liquid agent supplied by the manufacturer for coating surfaces to which
             the silicone rubber should adhere; e.g. the edges of  the metal strip sometimes embedded
             in pipes (Figure D.l), which are thus constrained to oscillate in 2-D. A  ‘releasing agent’
             is  also available, for coating surfaces on which the silicone rubber should not adhere at
             all, e.g. the inner surface of  the mould and the middle length of  the metal strip. In what
             follows, we  shall continue using the moulding of  a pipe as an example; a few words on
             other structures are given in Section D.2.
               Five basic pieces of  equipment are required: (i) the mould; (ii) a large injector syringe;
             (iii) a vacuum pump; (iv) a supply of compressed air; (v) a temperature-controlled oven
             (optional).
               A  schematic  of  a  mould  for  a  pipe  with  an  embedded  metal  strip  is  shown  in
             Figure D.2(a). It is basically composed of (a) a split outer mould and (b) a split cylindrical
             core (or, when no metal strip exists, a whole cylinder). The outer mould is made of  two
             solid-block halves; after the interfaces are ground flat, semicircular grooves are carefully
             milled in each with a ball end-mill, so as to produce a fine finish. Similar care should be
             taken to make sure that the split core when sandwiching the metal strip is cylindrical and
             of  the  required  diameter.  The  mould  can  be  made  of  Plexiglas  to  allow viewing  while
             casting or, for better  dimensional  tolerances  and robustness,  of  brass. The alignment of


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