Page 259 - Analytical method for food addtives
P. 259

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                                           refrigerator. Filter through glass fibre filter with KCl wash
                                                 M NaOH, using phenolphthalein
                                             solution. Place glass fibre filter and precipitate in beaker
                                               and wash with water. Heat solution to boiling point and
                                         alcohol to filtrate. Cool on ice bath. Stand overnight in
                                       Add tartaric acid solution followed by CH 3 COOH and
                                                 titrate while hot with 0.1
                                                 NaOH using phenolphthalein and add
                                             for 10 min, filter and transfer filtrate
                                           Shake, add 2 % HCl and KCl. Stand
                                                   5.2 mL in excess. Dilute to volume
                                         vigorously then 2 % Na 2 C 2 O 4  soln.
                                               M
                            M NaOH, add  7 Decant onto filter paper in Buchner funnel. Wash precipitate 3 times with alcoholic KOH solution. Transfer precipitate and filter paper to beaker, wash Buchner with hot water, heat to boiling point and titrate hot solution  M NaOH  with 0.1  E334–7, E354: L-tartaric acid and its salts  171
                            Neutralise with 1 tartaric acid, acetic acid and KCl. Add alcohol, stir until precipitate forms and refrigerate for 15 H  Add hot water to sample shaking  to vol flask. Neutralise with 1  with water. Stand and filter  Bitartrate method
                                                        Fruits and fruit

                            Wines      Cheese             products






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