Page 109 - Fiber Fracture
P. 109

94                                                            M.-H. Berger

                             2.5  fiNex. 610
                                   Saffil-Safimax   Nex. 720.   Nex. 440
                              2  -.     m
                          h                       Altexm        Nex. 480 I
                          m
                          Q                                    Nay312
                          9.
                             1.5  IPRD166
                          5
                          c      a FP
                              1  HAlmax
                          m
                          -
                          .-
                          a,
                          m
                          $  0.5  --
                          I-
                              07
                                 0      5      10    15     20     25     30
                                             Silica Content (wt%)
               Fig. 4. Evolution  of  the  room temperature tensile strength as a  function of  the silica content. The lower
               strengths of pure alumina FP and Almax  fibres are induced by their larger grain sizes of 0.5 Fm, in contrast
               to Nextel 610 and silica-containing alumina fibres.























               Fig. 5.  Typical  room  temperature  fracture  morphology  of  an  alumina  fibre  containing  silica  addition.
               Fracture has been initiated from a surface flaw, which can not be identified by SEM, located at the centre of
               a mirror zone.


               a-ALUMINA FIBRES

               Single Phase a-Alumina Fibres

                 To  increase the  creep resistance alumina fibres, intergranular silicate phases have
               to be reduced drastically. This imposes processes other than the addition of  silica to
               control a-alumina  growth. A pure a-alumina fibre was first produced by  Du  Pont in
               1979 (Dhingra, 1980). ‘Fiber FP’ was obtained by the addition, to an alumina precursor,
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