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4.1 Experimental 91
4.2 Theory 92
4.3 Uncertainties or Errors of Measurements 94
4.4 Example 95
5. Volumetric – Calorimetric Measurements
The Sensor Gas Calorimeter (SGC) 97
5.1 Experimental 99
5.2 Outline of Theory and Calibration 103
5.3 Example 106
6. Pros and Cons of Volumetry / Manometry 109
6.1 Advantages 109
6.2 Disadvantages 109
7. List of Symbols 111
References 114
Chapter 3: GRAVIMETRY 117
1. Introduction 117
2. Gravimetric Measurements of Pure Gas Adsorption
Equilibria (N = 1) 120
2.1 Two Beam Balances 120
2.1.1 Experimental 120
2.1.2 Theory 122
2.1.3 Uncertainties or Errors of Measurements 127
2.2 Single Beam Balances 129
2.2.1 Experimental 129
2.2.2 Theory 131
2.2.3 Uncertainties or Errors of Measurements 134
2.3 Examples 135
3. Thermogravimetry 153
4. Gravimetric Measurement of Multicomponent Gas
Adsorption Equilibria (N > 1) 157
4.1 Experimental 157
4.2 Theory 158
4.3 Uncertainties or Errors of Measurement 161
4.4 Examples 162
5. Pros and Cons of Gravimetry 167
5.1 Advantages 167
5.2 Disadvantages 170
6. List of Symbols and Abbreviations 171
References 175