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60                                      Multidimensional Chromatography

                                                                                          Two-dimensional separation of dimethylnaphthalenes in crude oil using a 50 m methyl (95%)/phenyl (5%) polysiloxane primary
                                                                                            column and a 50 m methyl (50%)/phenyl (25%)/cyanopropyl (25%) polysiloxane secondary column. The top trace indicates the primary separation














































                                                                                                107 (20). while the following chromatograms indicate individual heart-cut secondary analysis. Reproduced from R.G. Schäfer and J. Höltkemeir,


                                                                                                260,
                                                                                                1992,




                                                                                          Figure 3.4  monitor,  Anal. Chim. Acta,
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