Page 191 - Shale Shakers Drilling Fluid Systems
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174   SHALE SHAKERS AND DRILLING FLUID SYSTEMS



        Determine the Density of Drilled Solids                   4. Determine the weight of drilling fluid in the
                                                                     dish by subtracting the weight of the dish
            1. Select large pieces of drilled solids from the        from combined weight of the dish and drill-
               shale shaker and wash with the liquid                 ing fluid.
               phase of the drilling fluid (use water for         5. Divide the weight of drilling fluid in the dish
                                                                                  O          O
               water-based drilling fluid, oil for oil-based         by the density of drilling fluid (step 1). This
               drilling fluid, or synthetics for synthetic           is the volume of drilling fluid.
               drilling fluid)                                    6. Dry the material in the dish in an oven at
            2. Grind the drilled solids and dry in an oven           250°F for at least four hours.
               or retort                                          7. Weigh the dish containing dry solids
            3. Weigh the assembled, dry pycnometer                8. Subtract the dish weight from the weight of
            4. Add the dry drilled solids to the pycnometer          the dish containing the dry solids. This is
               and weigh                                             the weight of solids.
            5. Add water to the drilled solids in the pyc-        9. Divide the weight of dry solids (step 8) by the
               nometer, pressurize, and weigh                       weight of drilling fluid in the dish (step 4).
            6. Determine the water temperature                      This is the weight fraction of solids in the
            7. Determine the water density                          drilling fluid.
            8. Subtract the weight of the dry pycnometer         10. Subtract the weight of dry solids (step 8)
               from the weight of the dry pycnometer con-            from the weight of drilling fluid in the dish
               taining the dry drilled solids. This is the           (step 4). This is the weight of liquid in the
              weight of drilled solids.                             drilling fluid.
            9. Subtract the weight of the dry pycnometer         11. Divide the weight of liquid in the drilling
               containing drilled solids from the weight of         fluid (step 10) by the density of the liquid
               the water, drilled solids, and pycnometer.           phase of the drilling fluid. This is the vol-
              This is the weight of water added to the              ume of the liquid phase.
              pycnometer.                                        12. Subtract the volume of the liquid phase
           10. Divide the weight of the water (determined            (step 11) from the volume of the drilling
               in step 9) by the water density. This is the         fluid (step 4). This is the volume of solids
              volume of water added to the pycnometer.              in the drilling fluid.
           11. Subtract the volume of the water added to         13. Divide the volume of solids in the drilling
              the pycnometer (step 10) from the volume              fluid (step 12) by the volume of drilling
               of the pycnometer. This is the volume of             fluid. This is the volume fraction of solids
              drilled solids contained in the pycnometer.           in the drilling fluid.
           12. Divide the the weight of drilled solids           14. Multiply the volume fraction of solids in the
               (step 8) by the volume of drilled solids             drilling fluid by 100 to obtain the volume
               (step 11). This is the density of the drilled        percent of solids in the drilling fluid
              solids. This may be used in the previous
              equations to determine the volume percent       Sample calculation. While drilling a relatively
              of drilled solids in the drilling fluid.        uniform 2,000-foot shale section, a 200 x 200
                                                              mesh continuous screen cloth is mounted on a
          The pycnometer may also be used to more             linear shale shaker. An 11.2 ppg, freshwater, gel/
        accurately determine drilled solids in the drill-     lignosulfonate drilling fluid is circulated at 750
        ing fluid:                                            gpm while drilling. Given these parameters, the
                                                              following determinations can be assumed.
            1. Determine the density of the drilling fluid      Large pieces of shale are removed from the
              with the pycnometer                             shaker screen and the excess drilling fluid is washed
              a. Weigh the pycnometer filled and pres-        from the surface with distilled water. The shale
                 surized with drilling fluid                  pieces are ground and dried in a 250°F oven over-
              b. Subtract the weight of the dry pycno-        night. The shale is placed in a 173.91 cc pycno-
                 meter from the weight of the filled, pres-   meter and weighed. Water is added to the pyc-
                 surized pycnometer                           nometer and pressurized to approximately 350 psi.
              c. Divide weight of drilling fluid in pycno-    The increase in weight of the pycnometer deter-
                 meter by the volume of the pycnometer.       mines the volume of water required to fill the
                 This is the density of the drilling fluid.   pycnometer. (Room and water temperature is 68°F,
            2. Weigh a metal or heat-resistant glass dish     therefore, the density of water is approximately 1.0
            3. Add a quantity of drilling fluid to the dish   gm/cc.) Subtracting this volume of water from the
              and weigh                                       known volume of the pycnometer calculates the
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