Page 57 - Analytical method for food addtives
P. 57

hydrokinetic mode, loading 1s.
                                                       ºC. Injections in
                                                     phosphate buffer (pH 1.9) at
                                                       kV and 35
                                                       20
                                Sample preparation/extraction Reference Detection Method conditions  1 Photodiode HPLC: ODS-2 column with Sample dissolved in distilled water used  array at mM pentane- gradient of 5 as is for HPLC method.  nm  275 sulphonic acid in MeOH–H 2 O For CE filtered through 2 µm syringe (5:95) [A] and MeOH [B] filter before a
                            Summary of methods for caramel (class III)



















                            Table 4.1  Matrix  Method  Caramels IP-HPLC  followed  by CE
   52   53   54   55   56   57   58   59   60   61   62