Page 90 - Analytical method for food addtives
P. 90

Analytical methods for food additives
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                            Extent of validation Reference Statistical parameters  5 Linear range (µg/mL) 0.5–100 (FID), 2–500 (MS) (n=3) Precision of method LOD (µg/mL) 0.2 (FID), 1.0 (MS)  RSD (%) 3.7 (FID), 4.0 (MS) established and applied Checked with real samples for 5 samples of each analysed in triplicate to real samples  % n=15), mg/kg (RSD 3













                            Matrix  Fatty foods  Beverages and  jams  Foods  Beverages  Foods



                        Table 6.2 cont’d  Method  GC  HPLC  GC  HPTLC  GC–MS (SIM)
   85   86   87   88   89   90   91   92   93   94   95