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P1: JPJ/FFX  P2: FCH/FFX  QC: FCH/FFX  T1: FCH
            0521820928c08  CB644-Petlyuk-v1                                                      June 11, 2004  20:20





                        320    Synthesis of Separation Flowsheets

                               c. Which segments of component order are included in the trajectory tear-off
                                 segment Reg t(2)  of the top section?
                                            r
                               d. Can component 2 be the top or the bottom product? If not, then why?
                               e. Can mixture 1,2 be the bottom product? If not, then why?
                               f. Can trajectory tear-off points Reg t(2)  of the intermediate section of a column
                                                               m
                                 of extractive distillation be located at edge 1-2? If not, then why?
                           2.  Let the following segments of order of components 12435, 12345, 12354 (edge
                               1-2), and 12435, 21435, 21345 (edge 1-3) be located in the direction from vertex 1
                               at edges 1-2 and 1-3.
                               a. Can component 1 be the top product?
                               b. Can mixture 1,2 be the top product?
                               c. Can mixture 1,2,3 be the top product?
                                                                                              t
                               d. Which vertexes of triangle 1-2-3 does the trajectory tear-off region Reg of the
                                                                                              r
                                 top section join if mixture 1,2,3 is the top product?
                                                         (2)
                           3.  LetthefollowingsegmentsReg   oforderofcomponents:13452,14352,and14325
                                                         ord
                               be located in direction from vertex 1 to vertex 2 at edge 1-2 of the concentration
                               pentahedron.
                               a. Can component 1 be the top product?
                               b. Can component 2 be the bottom product?
                               c. Can the trajectory tear-off region Reg (2)  of the intermediate section of the
                                                                   m
                                 column of extractive distillation be located at edge 1-2? If yes, then why? Which
                                 component can be the top product, and which component can be the entrainer
                                 if the top product and the entrainer are one-component?


                               References

                               Abu-Eishuh, S. I., & Luyben, W. L. (1985). Design and Control of Two-Column
                                 Azeotropic System. Ind. Eng. Chem. Process Des. Dev., 24, 132–140.
                               Agrawal, R. (1996). Synthesis of Distillation Column Configurations for a Multi-
                                 component Separation. Ind. Eng. Chem. Res., 35, 1059–1071.
                               Agrawal, R., & Fidkowski, Z. T. (1998). Are Thermally Coupled Distillation Col-
                                 umn Always Thermodynamically More Efficient for Ternary Distillations? Ind.
                                 Eng. Chem. Res., 37, 3444–54.
                               Agrawal, R., & Fidkowski, Z. T. (1999). New Thermally Coupled Schemes for
                                 Ternary Distillation. AIChE J., 45, 485–96.
                               Avet’an, V. S., Petlyuk, F. B., & Serafimov, L. A. (1973). Optimal Design Three-
                                 Columns of Separation Unit of Lowest Carbon Acids with Water. In The
                                 Optimal Design in Refining and Chemical Industry.3,pp. 127–137. Moscow:
                                 VNIPIneft (Rus.).
                               Balashov, M. I., & Serafimov, L. A. (1984). Investigation of the Rules Governing
                                 the Formation of Regions of Continuous Rectification. Theor. Found. Chem.
                                 Eng., 18, 360–366.
                               Balashov, M. I., Grishunin, V. A., & Serafimov, L. A. (1970). The Rules of Con-
                                 figuration Boundarys of Regions of Continuous Distillation in Ternary Sistems.
                                 Transactions of Moscow Institute of Fine Chemical Technology,2,121–6 (Rus.).
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