Page 237 - Gas Wettability of Reservoir Rock Surfaces with Porous Media
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Application of Gas Wettability CHAPTER 6                  221




              Table 6.13  Core Permeability With Different Injection Core Volume
                          Multiples

              Injection Pore Volume Multiple             Permeability
                                           A     FSJ-03 KCl    NH 4 Cl ②    ③
              0                            41    37.4    44.9  50.7   49    35
              10                           41.1 37       43.2  49.6   41.7  32.7
              20                           41.7 37.6     37.4  41.8   40    30.1
              40                           40.1 35.9     34    40     36.1  28
              60                           39    34.8    33    36.5   34.6  27
              Maximum decreased            4.87 6.95     26.50 28.0   29.38 22.85
              permeability (%)


              6.3.2.1.3   Experimental Method of Core Flow
              Based on the interplanar spacing data of montmorillonite, each sample was
              prepared with the optimum concentration value. First, the initial permeability
              of rock samples was measured with standard brine, and each sample was
              injected with around 4PV. It was stable after being let to stand for 1 hour at

              60 C, and then the permeability of cores was measured with distilled water,
              when different pore volume multiples were injected, as shown in Table 6.13.
              Table 6.13 shows that the permeability of all the cores tended to decline when
              injected pore volume multiples increased, but the declining range of core per-
              meability of A was minimum. Therefore, as seen in Table 6.12, the antiswel-
              ling effect of A is the best, so trapezoid protection agent A was selected.



              6.3.2.2 COMPATIBILITY EVALUATION
              6.3.2.2.1   Evaluation of Compatibility Between Trapezoid
              Protective Agent A and Water Formation and Modification
              As the trapezoid protection agent is used in injected water, the compatibility
              with fluids formed and injection water must be good in the first place. The
              water formation and modification were screened with a 0.22 μm filter, at
              room temperature and optimum formation temperature.
              Dry and clear test tubes were used. First, 20 mL formation or modification
              water was added in every test tube, and then 2 mL of trapezoid protection
              agent A (at 10% concentration) was added. The tubes were stirred until the
              liquids mixed evenly. In order to facilitate observation, blank samples were
              used for comparison.

              The mixture was allowed to stand at room temperature for 4 hours, and com-

              patibility was observed. The mixture was then heated in a water bath at 90 C,
              for 4 hours. Observe and record the results, as shown in Table 6.14.
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