Page 32 - Handbook of Materials Failure Analysis
P. 32

CHAPTER


                  Engineering failure analysis

                  in chemical process                                       2

                  industries



                                                      Kashif M. Deen* and Ijaz H. Khan* ,†,{
                    Corrosion Control Research Cell, Department of Metallurgy & Materials Engineering, CEET,
                                                                                    *
                                                      University of the Punjab, Lahore, Pakistan
                                                                                    †
                    Institute of Chemical Engineering & Technology, University of the Punjab, Lahore, Pakistan


                  CHAPTER OUTLINE
                  1  Introduction ....................................................................................................... 26
                  2  How to Conduct Failure Investigation ................................................................... 30
                     2.1 Understanding the Problems ...............................................................30
                     2.2 Onsite Investigation ............................................................................31
                     2.3 Selecting the Samples ........................................................................31
                     2.4 Execution of Laboratory Testing ...........................................................31
                     2.5 Compiling the Data ............................................................................32
                     2.6 Drawing Conclusion ............................................................................32
                     2.7 Suggesting Remedies .........................................................................33
                  3  Case Studies ...................................................................................................... 33
                     3.1 Study of a Spent Caustic Drainage Line Pipe Failure in an Oil
                         Refinery ............................................................................................33
                         3.1.1  Background .............................................................................33
                         3.1.2  Brief Description of Process and Experimentation .........................34
                         3.1.3  Visual Observations and Testing .................................................36
                         3.1.4  Critical Review of Process Design ...............................................37
                         3.1.5  Analysis of Solutions .................................................................37
                         3.1.6  Electrochemical Testing .............................................................37
                         3.1.7  Conclusions .............................................................................38
                         3.1.8  Recommendations ....................................................................39
                     3.2 Failure of Plate Heat Exchanger due to Pitting ...................................... 39
                         3.2.1  Background .............................................................................39
                         3.2.2 Analytical Approach ..................................................................39
                         3.2.3 Description of Process ..............................................................41


                  {
                  The author has been died on January 03, 2015.
                  Handbook of Materials Failure Analysis With Case Studies from the Chemicals, Concrete, and Power Industries.  25
                  http://dx.doi.org/10.1016/B978-0-08-100116-5.00002-8
                  Copyright # 2016 Elsevier Ltd. All rights reserved.
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