Page 66 - Modern Analytical Chemistry
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1400-CH03  9/8/99  3:51 PM  Page 49






                                                                     Chapter 3 The Language of Analytical Chemistry  49


                                                          Start





                                                      Standardization



                                                                                Identify
                                                                      No
                                                         ICV, ICB                and
                                                          OK?                   correct
                                                                               problem
                                                             Yes


                                                                      No
                                                        CCV, CCB
                                                          OK?


                                                             Yes

                                                         Run 10
                                                         samples
                                                                             Discard results
                                                                              for last set of
                                                                               samples
                                                                      No
                                                        CCV, CCB
                                                          OK?


                                                             Yes


                                                  Yes     More
                                                        samples?


                                                             No


                                                          End


                 Figure 3.7
                 Schematic diagram of a portion of the Contract Laboratory Program protocol for the analysis of trace metals by graphite furnace atomic
                 spectrophotometry, as specified by the Environmental Protection Agency. (Abbreviations: ICV = initial calibration verification; ICB = initial calibration blank,
                 CCV = continuing calibration verification, CCB = continuing calibration blank)
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