Page 154 - Advances in Forensic Applications of Mass Spectrometry - Jehuda Yinon
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1522_C03.fm  Page 137  Thursday, November 13, 2003  9:53 AM











                              RT: 8.12 - 14.00 SM: 7G
                               100                                                   NL:
                                95                             RT: 11.05             4.55E3
                                90                                                   TIC F: + c El
                                85                                                   SRM ms2
                                80                                                   435.20@-4.00 [
                                75                                                   208.49-209.11]
                                70                                                   MS meth02041
                              Relative abundance  60
                                65
                                55
                                50
                                45
                                40
                                35
                                30
                                25
                                20
                                15
                                10
                                5
                                0
                               100                                 RT: 11.40         NL:
                                95                                                   5.74E2
                                90                                                   TIC F: + c EI
                                85                                                   SRM ms2
                                80                                                   446.20@-4.00 [
                                75                                                   194.49-208.11]
                                                                                     MS meth02041
                                70
                                65
                                60
                                55
                                50
                                45
                                40
                                35
                                30
                                25
                                20
                                15
                                10
                                5
                                0
                                     8.5  9.0  9.5  10.0 10.5 11.0 11.5 12.0 12.5 13.0 13.5
                                                          Time (min)

                             Figure 3.4  MS/MS-single reaction monitoring (SRM) mass chromatograms of
                             a 100-mg hair specimen of a bodybuilder, revealing the presence of methenolone.
                             (Reprinted from Kintz, P. et al., J. Chromatogr. B, 766, 161, 2001. Copyright 2001,
                             with permission from Elsevier Science.)




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