Page 141 - Analytical method for food addtives
P. 141

17
                                                              Fluorescence
                                                                  nm
                                                                nm
                                                                  em 470
                                                                ex 400
                                                                    acetic acid in 700 mL
                                                                tetrabutylammonium
                                                              g 40 % aqueous
                                                                  g
                                                                  hydroxide and 3
                                                                      water
                                                              34
                                                              Whatman C8
             To 1 mL sample, previously treated  21 The SO 2  evolved was swept by a stream of nitrogen to a gas infrared cell. The flow injection (FI) recordings were M KOH at 30 ºC, with 0.5 mL 1 registered and the analytical variable was the area of the M H 2 SO 4  was added 0.5 mL 3.4 co-added spectra obtained, in wave number range 1429 and cm –1
                                                              Blended with buffered formaldehyde
                                                                solution. SPE clean-up on RP C18
             Musts and wines  Grape juice        Matrix  Foods and  beverages  Foods  columns






                              Comparison of 5  methods including  distillation,  iodimetric and  enzyme-based  chromatographic



             FTIR                            (b)  Method  Ion  exclusion  IEC–EC  HPLC
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