Page 235 - Analytical method for food addtives

Carrier gas N 2 at 4 mL/min
programmed 140–300 ºC.
mm,
m × 0.53
1.5 µm)
(30
ether and 0.2 % tetradecanol added and
60–80 mg oil sample and vortex-mixed
for 20 min methylation. Extracted with
mixed thoroughly. 0.3 µL ether layer
Summary of methods for BHA in foods Reference Detection Conditions Column Sample preparation/extraction 1 FID at 210 ºC Injection size 3.0–9.0 µL, 2 columns: QF-1 and Ground sample placed in chromato- flash heater 200 ºC, N 2 flow Apiezon L/gas-chrom graphic column and eluted with CS 2 , rate: 40 mL/min for Apiezon Q at 160 ºC

Table 12.1 (a) Matrix Method Cereals GC Fatty foods GC Foods GC–MS (SIM) Edible fats GC and oils