Page 179 - Failure Analysis Case Studies II
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                 Fig. 6.  Fracture surfaces of bolts 19 and 20, showing areas of fatigue from multiple origins (arrowed).



           6.2.  Scanning electron microscopy
            The fracture surface of bolt  20, which  showed a  typical area  of fatigue, was examined using
           scanning electron microscopy. At low magnification, the extent of the corrosion could be clearly
           observed, with the origins of fatigue crack initiation corresponding to corrosion pitting in the thread
           root. At high magnification, features typical of fatigue propagation were observed (Fig. 9).

           6.3. Optical microscopy
            Longitudinal  sections were cut from bolts  3,  17 and 31, and prepared  for optical microscopy
           using standard metallographic procedures.
            In the unetched condition, the steel from which the bolts were manufactured  was relatively free
           from  non-metallic  inclusions. Etching  in  2%  nital  revealed a  fine,  tempered  martensite  micro-
           structure for each bolt, and no evidence of surface defects such as decarburization (Fig. IO).


                      Table 1.  Area of fatigue crack growth relative to the cross-sectional area of each bolt
            Bolt no.   Percentage area of fatigue      Bolt no.   Percentage area of fatigue
                           30                            11           20
                          < 10                           18           15
                           15                            19           10
               4           15                            20           10
               5           20                            21           15
                          < 10                           22          10-15
                            0                            23           20
                           10                            24          < 10
               9           20                            25          < 10
              10           15                            26           30
              11          < 10                           21           20
              12           10                            28            0
              13           20                            29           10
              14           10                            30           15
              15           20                            31           10
              16           20                            32           20
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