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Failure Analysis Case Studies II
                     D.R.H. Jones (Editor)
                     0 200 1 Elsevier Science Ltd.  All rights reserved                      313






                                   CORROSION  OF  FLEXIBLE  WAVEGUIDES


                                   D. PAPATHEODOROU, M. SMITH and 0. S. ES-SAID*
                           Mechanical Engineering Department, Loyola Marymount University, 7900 Loyola Blvd, Los Angeles,
                                                   CA 90045-8145, U.S.A.
                                                   (Received 9 August 1997)

                         Abstract-Waveguides   are  commonly  used  in  spacecraft  subsystems to  convey  signals.  After  noticing  a
                         transponder ouput power drop, borescope inspection of a flexible waveguide revealed a green contaminating
                         residue on silver plated brass and copper sections. Analysis revealed that the residue, primarily copper hydroxy
                         nitrate, Cu(OH),N03, was created by  exposure of the plating  to nitric acid. Possible  sources of nitric acid
                         include inadequate cleanliness after parts were exposed to a nitric acid containing silver bright dip, or high
                         temperature electrical arcing in the presence of air and moisture. Whatever its source, it is suggested that the
                         waveguide be plated with a more corrosion resistant metal such as rhodium. 0 1998 Elsevier Science Ltd. All
                         rights reserved.
                         Keywords: Corrosion, electronic-device failures, surface coatings.


                                                  1.  INVESTIGATION

                     Flexible waveguides, common in spacecraft payload sub-systems, transport signals between various
                     units (e.g., filters, transponders, and converters). During preliminary testing at ambient temperature
                     and pressure, an output power drop was detected within a signal generating unit of a waveguide
                     system. Green contamination  residue was found in the waveguides. An investigation commenced
                     to characterize the corrosion and determine its cause.
                      The flexible waveguide, Fig. 1, has a rectangular thin wall cross section having corrugations which
                     allow it to be formed. The green residue was found on brass and copper surfaces, primarily in the
                     bottom of those corrugations (dark bands in Fig. 2). In some areas, the waveguide wall had corroded
                     through.
                      To determine the material damage severity, as well as the composition of the residue, an analysis
                     of samples taken from the waveguide was conducted using visual inspection, optical microscopy,
                     scanning electron microscopy and X-ray methods. Samples were prepared by cutting and spreading
                     open the waveguide to expose its internal surfaces containing many voids and much debris (Fig. 3).



















                                Fig. 1. Profile of waveguide. Dark bands are low points in waveguide or corrugations

                      *Author to whom correspondence should be addressed.
                    Reprinted from Engineering Failure Analysis 5 (l), 49-52 (1998)
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