Page 5 - Multidimensional Chromatography

CONTENTS

List of Contributors xi

Preface xiii
PART 1: GENERAL 1
1 Introduction 3
K.D. Bartle
1.1 Preamble 3
1.2 Packed Capillary Column and Unified Chromatography 4
1.3 Resolving Power of Chromatographic Systems 6
1.4 Two-Dimensional Separations 9
1.5 The Origins of Multidimensional Chromatography 12
Acknowledgements 13
References 13
2 Coupled High Performance Liquid Chromatography with High
Resolution Gas Chromatography 17
L. Mondello
2.1 Introduction 17
2.2 Transfer Techniques 18
2.3 Vaporization with Hot Injectors 25
2.4 Transfer of Water-Containing Solvent Mixtures 28
2.5 Indirect Introduction of Water 31
2.6 Conclusions 38
References 42
3 Multidimensional High Resolution Gas Chromatography 47
A. C. Lewis
3.1 Introduction 47
3.2 Practical Two-Dimensional Gas Chromatography 48
3.3 Practical Examples of Two-Dimensional Chromatography 57
3.4 Conclusions 72
References 72
4 Orthogonal GC–GC 77
P. J. Marriott
4.1 Introduction to Multidimensional Gas Chromatography 77
4.2 Introduction to GC GC Separation 80