Page 40 - A Practical Introduction to Optical Mineralogy
P. 40

THE  MICROSCOPIC STUDY  OF MINERALS                                       THIN- AND POLISHED-SECTION  PREPARATION

                         crossed polars it should have four extinction positions at 90°,  and the   (3)  Grinding the surface fiat using carborundum grit and water on a
                         polarisation colours seen in each quadrant should be identical. Adjust        glass or a  metal surface.
                         the  polariser  and  analyser  until  the  best  results  are  obtained  (see   ( 4)  Polishing the surface using diamond grit and an oily lubricant on a
                         Hallimond  1970, p.  101).                                                    relatively  hard 'paper'  lap.
                           Ensure that the stage is well centred using the high power objective    (5)  Buffing  the surface  using  gamma  alumina  powder and  water as
                         before studying optical figures.                                              lubricant on a  relatively soft 'cloth'  lap.
                                                                                                   There  are  many  variants  of  this  procedure,  and  the  details  usually
                         1.11  Thin- and polished-section preparation                              depend on the nature of the samples and the polishing materials, and
                                                                                                   equipment that happen to be available. Whatever the method used, the
                         Thin sections are prepared by cementing thin slices of rock to glass and   objective  is  a fiat,  relief-free, scratch-free polished surface. The tech-
                         carefully grinding using carborundum grit to produce a paper thin layer   nique  used  by  the  British  Geological  Survey  is  outlined  by  B.  Lister
                         of rock.  The standard  thickness of 30 microns  is  estimated using  the   (1978).
                         interference colours of known  minerals in  the section.  A  cover slip  is
                         finally  cemented on top of the layer of rock  (Fig.  1.11).
                          The three common types of polished section are shown in Figure 1.11.
                         Preparation of a  polished surface of a  rock or ore sample  is  a  rather
                         involved  process which  involves five  stages:

                         (1)  Cutting  the sample with  a diamond saw.
                         (2)  Mounting  the sample on glass or in  a cold-setting resin.
             Figure 1.11   Thin section                 Polished block
             Sections.
                                                        polished surface
                          ~~



                                           glass sltdc
                          rock slice
                          30 IJ.m  thick         rock slice
                                                 -50  mm thick
                                                                resin  block

                          Polished thiri section          Polished wafer or doubly
                                                          polished section
                               polished surface   glass slide     resin cage
                          ~


                                                rock slice
                           rock slice           50--500  IJ.m  thick
                           - 30 IJ.m  thick
                                                         polished surfaces
                              3cm

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