Page 88 - Adsorption, Ion Exchange & Catalysis- 2007, Elsevier - Copy
P. 88

Else_AIEC-INGLE_cH003.qxd  7/13/2006  1:45 PM  Page 84
                    84                               3. Heterogeneous Processes and Reactor  Analysis


                    unbaffled tank but a vortex creates problems, partial-length baffles may be used. These are
                    of standard width and extend downward from the surface into about one-third the liquid vol-
                    ume. In the region of laminar flow (  N  Re  < 10), the same po wer is consumed by the impeller
                    whether baffles are used or not, and the The flo  y are not usually required. w pattern may be
                     .
                     When the
                    affected by the baf but not alays adv the baf antageously w y are needed,  fles
                    fles,
                    are usually placed one or two widths radially off the tank w to allow fluid to circulate all,
                    behind them and at the same time produce some axial deflection of flow.
                    3.3.2 Mixing in gas–solid systems

                    Batch reactors
                    To ensure complete and uniform mixing conditions of the fluid throughout the reactor in ,
                    such systems, a special design is required. Such a design has been presented by Levenspiel
                    (1972) and it is shown in Figure 3.22.
                      ,
                      In this type of reactor an agitator is used for mixing the fluid in the main body of the
                    vessel, whereas the gas is rapidly circulated throughout the reactor and forced to flo w
                    through the catalyst bed. A low conversion per pass through the catalyst is required so that
                    uniform composition in the reactor is achie ed. v
                    s eactor Continuous flow r
                    ol- ed-flow reactor requires uniform composition of the fluid phase throughout the v A mix
                    ume while the fluid is constantly flowing through it. This requires a special design in order
                    v to be achieed in the case of gas–solid systems. These reactors are basically e xperimental
                    devices, which closely approach the ideal flow conditions and have been devised by Carberry
                    (Levenspiel, 1972). This device is called a “basket-type mix (Figure 3.6). The ed reactor”
                    catalyst is contained in four rapidly spinning wire baskets.













                                                Rapid circulon of gas i at  catalys  t



                                          gas




                                       Figure 3.22  Mixing in gas–solid batch reactors.
   83   84   85   86   87   88   89   90   91   92   93