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132                              Advances in Eco-Fuels for a Sustainable Environment




























         Fig. 5.2 Schematic layout of microwave pyrolysis setup. (1) Nitrogen cylinder. (2) Data
         acquisition system. (3) Magnetron. (4) Blower. (5) Quartz vessel. (6) Stirrer motor. (7) Control
         panel. (8) Water tank with pump. (9) Condenser. (10) Nitrogen flow regulator.





                TG (%)                                         DSC (mW/mg)
                                  Value: 211.2°C, 99.9%           exo
               100                                                 [1] 8
                                               Value: 465.5°C, 6.316 mW/mg
                                                                     7
                80                                                   6

                                                                     5
                                Value: 389.8°C, 56.2%
                60
                                                                     4
                                                    Value: 390.3°C, 4.145 mW/mg
                                                                     3
                40
                                                     Residual mass: 3.1% (597.7°C)
                                                                     2
                20                                                   1
                                                                     0
                                                                   [1]
                0
                        100     200      300      400     500
                 WEO                  Temperature (°C)

         Fig. 5.3 TGA and DSC curve for waste engine oil (WEO).
   156   157   158   159   160   161   162   163   164   165   166