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Topics Eds., Practice, 1997. 1968. IL, 1979. York, 1981. New Wiley, Derivatization Ronkonkoma, Pergamon

Special Grushka, E. and Theory NY, Rockford, New Amsterdam, and Chelates,

and (1994). Wiley, Wiley, Elsevier, Chromatography, Reagents, 61105. IL, Corp., Metal
Brown Chromatography: 844A 66, (1996). Practice, Chemical, Reactions, 60053. Chemical of

R. 143 for IL, Rockford,
P. Chem., and Pierce Chromatography, Derivatization Fluka
(37) Gas Anal. 733, A, Theory Derivatization of Derivatives GC Grove, Co., Agents, (1996). Chromatography
Chromatography (1990). Headspace J., Pawliszyn, Chromatogr. Microextraction: Compounds, Organic of Analytical Gas in Handbook Chromatography, Morton Inc., Chemical Pierce Silylating 19 733, Gas E., (1975). 303

Methods) in Advances 5. Chpt. 362 8, LC-GC, Static S., L. and J., M. J. K., Levsen, Phase (1990). 216 8, of Silylation Handbook Derivatization M., J. Gas Technologies, of Derivatization, J., Heberle, A, Chromatogr. R. Sievers, 113, Chromatogr.,

Sampling E. Z. 1997, NY, V., J. Ettre, and K., 1997. NY, Yang, Z., and R., Solid J., LC-GC, D., E., A. R., D. Chemical J., Halket, and K., 1993. Derivatization for Regis Chart, and G., 1995. J. H., and W., R. 1965. Oxford, J. J.,

(Special Penton, Dekker, Hinshaw, Bruno, Wiley, Zhang, Eiseret, Pawliszyn, Rood, (Derivatization) Pierce, Knapp, Drozd, Blau, York, Wall Handbook Simchen, NY, Kataoka, Mosier, Press, Drozd,

172 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31.