Page 98 - Basic Gas Chromatography
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Inlets   85  References      capillary   a   of  installation   the   are  required   are   that  changes   major   The   this   for   Kits  detector.   the   for   gas  make-up   of  addition   the   and  injector   ig   and  McMurtrey   and  houses,  supply   lab   from  available   are  purpose   on  one.  The  easiest  homemade   a  construction of   the  described   have   [13]   ]   [  Jennings   [14];  columns  wide-bore   to  columns  pa

   and                method         unsaturated   deactivate   acid   commer-   type;   in   but   difficulties   diame-   phases.   normal   achieve   samples;   columns;   columns   packed-column

   Columns   Application   acids   EPA   isomers   distillation   hydrocarbons,   used   to   phosphoric   available   important   discussed   decreases,   packing   with   inside   few   columns   and   to   volatile   packed   capillary   capillary



   Packed   Applications   Pesticides   Amino   Solvents   Phthalates,   Amines   gases  Sulfur   Xylene   Simulated   Light   Freons   hydroxide   is   amines   and   Most   are   another   are   they   diameter   of   the   columns   for   a   packed   are:   (a)   for  highly   normal   mixed  packing.   analyses,   use.  Older,   to   field   accept




         Special           (on   and              like   phenols.   Table   5.5.   are   and   column   because   Packed   available   normal   examples   (b)   with   a   of   COLUMNS   some   general   the   in   cost

         for        1500®   Deactivation   HPQ,   clay   C®   potassium   and   in   packings   columns   the   case   result.   commercially   Some   capacity;   possible   for   for   minimal
         Packings   OV-210®   Carbowax   QF-1®   for   KOH   1.5%   34®   Carbopack   B®   or   compounds   acids   listed   Chiral   capillary   as   special   that   between   needed.   sample   is   advantages   CAPILLARY   preferred   preferred   retrofitted   at


         Phase   1.95%   1%  OV-210®   0.1%   1.95%   reducers)   2%   +   +   Bentone   5%   B,   C   or   on   Carbopack   sodium   basic   free   like   columns   are   in   improves   a   drops   are   compromise   is   high   than   selectivity   are   are   be   can   them

        Stationary   Liquid  Phases   OV-17®   +   +   SP-2401®   +   +  OV-17®   (tail  Liquids   Apiezon   L®   Polyphenylether   +   Petrocol   A,   Picric   Acid   on   example,   for   used   columns.   used   Columns   performance   represent   pressure   micrometers   a   columns   and   speed   the   FOR   columns   and   upgrading



        5.5   Packing   Mixed   1.5%   OV-17®   2%   20%   1.5%   Mixed   10%   12%   PTFE)   in   SP-1200®   5%   10%   0.19%   Fluorcol   5%   For   packing   compounds   special   packed   often   diameters   high   750   when   tubular   efficiency   greater   obtain   packed   efficient   chromatographs   thereby
        TABLE   Column         Other                  Other   in   more   10.   Microbore   Column   the   of   used   for   to   UPGRADING   more
  34          A.       B.      C.              sites.   the   acidic   cially   are   ter   small   and   ters   are   open   high   (c)   (d)   While   are   gas   umns,






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