Page 99 - Basic Gas Chromatography

capillary for ig [ simple; ioniza- (1995). (1980). Chromatogr.
85 this on ] as are PA, NY, NY, Chap-

a Kits and Jennings columns flame Bellefonte, Dekker, Varian Associates, 21 1407 Dekker, 1987,
of one. The easiest rather These as Ed., [15], 27, and (1975). Ed., Diego, J. J.,
installation detector. McMurtrey [14]; is tubing. well as Supelco, 890, - Giddings, (1965). Chromatography, Lab. Am. 1402 52, 533 13, Giddings, (1983). San Press, R. Mathieu,

the the for and homemade columns conversion and [16] Bulletin C. J. 28, 1348 37, W., (1976). Chem. Sci., (1979). C. J. 28, 974 55, Academic and
are gas houses, a wide-bore The fittings detectors (1973). 136 Guide, Vol. Chem. Gas Wentworth, 799 48, Anal. M., Chromatogr. 594 51, Vol. Chem., E., A.
required make-up supply to detail. some 11, Sci., (1966). Anal. and Chem. M. J. J., J. Chem. Anal. (1985). Chromatography, Lawson,

are of lab construction of columns in are conductivity Application 309 Chromatography, Jr., E., S., Anal. H., Kopecni, Leary, Anal. Chromatography, J., T. 94 [10], M., B.
that addition from the procedure needs Chromatogr, Column 38, Chem., in A. Thompson, B., Fundamentals of Gas Analysis by Stearns, J. and J., and A., Apffel, in Knight, 17, Gas Gordon,
changes the available described packed from the one all thermal J. M., D. Packed Anal. L., Advances E., 2. Lawson, and M., 1977. CA, H., Cai, J., Purnell, and J., R. Laub, F., Palocsya, F., and L., Advances J., 3. and D., K. Lab, Am. L., Analytical W., H., C. (1978).

References major The and injector are purpose have [13] is version discussed has minimum, a with useable detectors. tion REFERENCES Ottenstein, . Anonymous, 1995. O. Hollis, . Willis, Chpt D. . 1989, J. Miller, . . Alto, Palo Madabushi, . R. Laub, . C. Chien, . D. Lynch, 10. R. Pecsok, 11. G. Price, 12. 1989, Chpt. McMurtrey, 13. M. Duffy,

Inlets for they Chap- very They both or col-

and method unsaturated deactivate acid commer- type; in but difficulties diame- normal samples; columns; columns packed-column
Columns Application acids EPA isomers distillation hydrocarbons, used to phosphoric available important discussed decreases, packing with inside phases. few columns and achieve to volatile packed capillary capillary

Packed Applications Pesticides Amino Solvents Phthalates, Amines gases Sulfur Xylene Simulated Light Freons hydroxide is amines and Most are another are they diameter of the columns for a packed are: (a) for highly normal mixed packing. analyses, use. Older, to field accept

Special (on and like phenols. Table 5.5. are and column because Packed available normal examples (b) with a of COLUMNS some general the in cost

for 1500® Deactivation HPQ, clay C® potassium and in packings columns the case result. commercially Some capacity; possible for for minimal
Packings OV-210® Carbowax QF-1® for KOH 1.5% 34® Carbopack B® or compounds acids listed Chiral capillary as special that between needed. sample is advantages CAPILLARY preferred preferred retrofitted at

Phase 1.95% 1% OV-210® 0.1% 1.95% reducers) 2% + + Bentone 5% B, C or on Carbopack sodium basic free like columns are columns. in improves represent a drops are compromise is high than selectivity are are be can them

Stationary Liquid Phases OV-17® + OV-17® + SP-2401® + + OV-17® (tail Liquids Apiezon L® Polyphenylether PTFE) SP-1200® + Petrocol A, Picric Acid on example, for used used Columns performance pressure micrometers a columns and speed the FOR columns and upgrading

5.5 Packing Mixed 1.5% 2% 20% 1.5% Mixed 10% 12% in 5% 10% 0.19% Fluorcol 5% For packing compounds special packed often diameters high 750 when tubular efficiency greater obtain packed efficient chromatographs thereby
TABLE Column Other Other in more 10. Microbore Column the of used for to UPGRADING more

34 A. B. C. sites. the acidic cially are ter small and ters are open high (c) (d) While are gas umns,

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