Page 368 - Chemical process engineering design and economics
P. 368
Separator Design 347
The HETS will then be higher then at the minimum point. To estimate the design
HETS, select an HETS that is 20% higher than the minimum value. Also, given in
Table 6.3 1 is the maximum volumetric efficiency, defined by Equation 6.31.
Vc+V D
T!V = ———— (6.31)
HETS
Karr and Lo [63] have developed simple scaling rules for the Karr extractor.
To scale HETS from one column size to another, requires that the plate spac-
ing, amplitude, and total volumetric flow rate per unit area be kept the same for
each extractor. They found for a high interfacial-tension system such as the o-
xylene, acetic-acid, water system, that
(HETS) 2 ( D 2y 38
————— = 1 —— I (6.32)
For a low interfacial-tension system such as MIBK, acetic acid, water, the expo-
nent is 0.36, only slightly different.
To scale the reciprocating frequency, they also developed the following rela-
tion.
0) 2 f D , V- 16
— = 1 —— I (6.33)
co, I D 2 )
Equations 6.31 to 6.33 have been successfully used to scale many Karr extractors
from pilot plant experiments to commercial scale extractors up to 1 .53 m (5.02 ft)
in diameter [61].
Copyright © 2003 by Taylor & Francis Group LLC