Page 386 - Design of Simple and Robust Process Plants
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9.5 Closed Loop Steady-state Optimization  373

                Vapor
                 load

                            Operational
                               area






                                          Liquid load
                Fig. 9.11. Constraints of a distillation column.





                Table 9.1. Constraints of simple distillation column.

                Process                Bottom temperature (decomposition)
                                       Top temperature (solidification)
                Column                 Design temperature
                                       Design pressure
                Internals              Flooding and weeping of top section and bottom section
                                       Gas loading (high and low)
                                       Liquid loading (high and low)
                                       Overload at feed section (high and low)
                                       Pressure drop
                Reboiler               Fouling
                                       Heat source temperature and pressure
                                       Design temperature and pressure. Shell and Tube
                Condenser              Fouling
                                       Cooling medium temperature and pressure
                                       Design temperature and pressure inside and outside
                Reflux drum            Design temperature and pressure
                Instrument measurements  Range
                Instrument actuators   Capacity/range
                Lines                  Design temperature and pressure
                                       Pressure drop
                Pumps                  Design temperature and pressure
                                       Capacity and head



                The final result of the model should be accurate and robust over the entire opera-
                tional range. The model must be tested in combination with the optimizer, and
                demonstrate its robustness from different starting points.
                  At the feasibility stage (Section 9.6.1), the factors that play an important role in
                the overall economic process performance are identified by sensitivity analysis. Also,
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