Page 198 - Failure Analysis Case Studies II
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           The failure cracks started from cold slugs or voids, because they occurred near the base of an
           adjacent buttress, which possessed a sharp corner with the sidewall, and represented a stress
           raising  factor  of  about  4.2. The cold  slugs and/or voids  were  more  serious  in  their  stress
           magnifying effect, possibly having a stress raiser of about 6, so the effective stress concentration
           in this zone was about 25 times the nominal applied stress of only I .55 MN mP2.
        3.  The final factor  which  made the situation critical was the presence of  a substantial level  of
           frozen-in strain, produced by cold moulding the material. This effectively added some 20 MN
           m-’  extra stress to the surface of the cold slug, producing a total stress in the region of about
           59 MN m-’,  a stress comparable with the mean strength of the material. Brittle cracks were
           thus initiated at the surface of cold slugs or voids when the system was first pressurised, and
           grew progressively at each use of the cooling system. The cracks had penetrated through to the
           interior of the radiator, but only small quantities of water leaked out under pressure, judging
           by the several traces of contaminant found near the crack. When the cracks reached a critical
           size, they propagated catastrophically, releasing pressure from the system, and hence resulted
           in loss of the cooling facility.
        4.  The failed specimen appears to be a maverick which was probably accidentally included in the
           batch sent to the car manufacturers. Normal QC procedures usually prevent such mouldings
           being used, but when this batch of tanks was moulded, they failed to catch the rogue product.
           Careful visual inspection  at the moulding machine would  probably  have  caught  the rogue,
           provided the operator was aware of what to look for in terms of defects such as weld lines and
           cold  slugs.  It is  a difficult product  to examine  quickly  for  such defects owing  to its  black
           colouration, which were only revealed by dusting with whiting and by very close visual inspec-
           tion.



        Acknowledgements

          Naomi Williams (OU) for SEM, Jim Moffatt (OU) for mechanical testing, Gordon Imlach (OU)
        for etching experiments, and the manufacturer for permission to publish this edited account of a
        more substantial report.


        References


        [I]  Lewis PR (Course Chair), Design and manufacture with polymers, T838. Post-graduate OU Course in the Manu-
           facturing Programme,  1998, Block 5.2, section 4:47.
        [2]  Lee SM, editor. International  encyclopaedia of composites. New York: VCH,  1990: for entry on Processing, void
           formation in melt flow thermoplastic composites, p. 302.
        [3]  International  encyclopaedia  of composites.  Op cit., for  entry  on Characterisation,  a  general  review covering X-
           radiography, OM and SEM.
        [4]  Folkes MJ, Russell DAM. Orientation  effects during the flow of  short-fibre  reinforced  thermoplastics. Polymer
           1980;21: 1252-1258.
        [5]  Peterson RE. Stress concentration  factors. John Wiley & Sons, Inc.,  1974, Fig 39; also in Pilkey WD, Peterson’s
           stress concentration factors 2nd ed. John Wiley & Sons, 1997, Chart 2.29.
        [6]  Peterson, op cit., Figure 150; Pilkey, op cit., Chart 4.71.
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