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10   Gas Purification

















                    Flexitray valve tray            Standard Flexitray valve















                 Sieve tray                           Bubble-cap tray
          Figure 1-2. Typical commercial trays. Courtesy of: Koch Engineering Company, Inc.



        Packed Columns

          Packed columns are gaining favor for a wide range of applications because of the develop-
        ment of packings that offer superior performance, as well as the emergence of more reliable
        design techniques. The most commonly used packing elements are packed randomly in the
        column. Non-random  ordered  (or structured) packings  were originally  developed  for small
        scale distillation  columns to handle difficult  separations. Their use has recently  expanded,
        however, and ordered packings  are now offered by several companies for large scale com-
        mercial applications. The current availability of performance data and rational design proce-
        dures makes  the use of ordered packing  worth  considering for cases requiring high  mass
        transfer efficiency and low pressure drop.
          Packed contactors are most frequently  used  with countercurrent  flow of liquid  and gas.
        However, in special cases they are used in a crossflow arrangement with the liquid flowing
        down through a bed of packing while the gas flows horizontally,  or in cocurrent flow with
        liquid and gas flowing in the same direction. Cocurrent contactors using structured packing
        elements similar to in-line  mixers  are used  for gas purification  applications  when a single
        contact stage is sufficient; for example, when an irreversible reaction occurs. They have the
        advantage of operating with much higher gas velocities than countercurrent designs without
        being subject to flooding problems.
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