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Measurement techniques: thermocouples 277

                                                        cu
             Readout
             instrument                \\\ ------- -
             types
             C.J. compensation                           /-
                                      cable                     Pt
                                                       Cu:Ni
             Figure 14.41 Thermocouple compensating cable
             14.5.3. IO  Accuracy consideration
                                                        In  carrying  out  these  calibrations  the  whole
             The  very  extensive use  of  thermocouples  stems   installation needs to be calibrated: thermocouple
             from  their  great  versatility combined  with  their   readout  instrument  together  with  compensating
             low cost. However, as seen in Table 14.13, thermo-   cable.  In  cases  where  very  high  accuracy  is
             couples  have  a  fairly  wide  permitted  tolerance.   required, compensating cable should not be used;
             This is due to the fact that most metals used for   the conductors should be thermocouple metal for
             thermocouples are alloys and it is not possible to   the full length of the installation.
             manufacture alloys to the same reproducibility as   There  is  on  the  market  some  very  versatile
             pure metals, It must be said that, in general, manu-   equipment  for thermocouple  calibration.  Typic-
             facturers  do manufacture  their thermocouples to   ally, the facilities provided include thermocouple
             better  tolerance  than  BS  4937  demands.  But,   simulation for types E, J, K. R. S, and T. thermo-
             where the highest accuracy is required, it is essen-   couple  output  measurement  with  cold  junction
             tial to calibrate thermocouples on installation and   compensation and resistance thermometer simu-
             to recalibrate them at regular intervals to monitor   lation. Tests can be static or dynamic using ramp
             any deterioration  due to corrosion or diffusion of   functions.
             foreign elements into the hot junction.    As  with  any  other  type  of  temperature  mea-
               Where high accuracy is required it is necessary   surement the location of the thermocouple junc-
             to calibrate first the thermocouple readout instru-   tions is critical. This is just as important for the
             ment and then the thermocouple itself in conjunc-   cold junction  as for the hot junction.  It must be
             tion with the instrument.                remembered that there may well be a temperature
               The  calibration  of  instruments  can  be  done   gradient  over quite  short distances in  an instru-
             with  a precision millivolt source which injects a   ment  and  unless  the  cold junction  temperature
             signal  equivalent  to  the  temperature  difference   sensor  is  in close thermal contact  with  the cold
             between  the  ambient  or  cold junction tempera-   junction  itself a  reading  error  of  several degrees
             ture and a temperature in the region in which the   Celsius may  result.  This problem  is  at its worst
             thermoccluple is to be used.             with mains electricity powered measuring instru-
               To  calibrate  or  check  thermocouples  the  hot   ments  where  there  is  a  certain  amount  of  heat
             junction must be kept at an accurately known tem-   liberated by the power unit.
             perature. This can be done by  inserting it into a   The point to remember is that it is not usually
             heated isothermal block. An isothermal block is a   adequate to measure  the  air temperature  in  the
             block of  metal: large compared with the thermo-   vicinity of the cold junctions. The sensor should
             couple  being  measured  and  made  of  copper  or   be in good thermal contact with them.
             aluminum. The block has provision for heating it   An  obvious point,  but one which surprisingly
             and in some cases cooling. It is well insulated from   often causes trouble, is the mismatch between the
             the environment and is provided with suitable holes   thermocouple and the measuring instrument. The
             for inserting various sizes of thermocouple. Where   obvious  mismatch  is  using  the  wrong  type  of
             not so high precision is required the thermocouple   thermocouple or compensating cable.
             can be immersed in a heated fluidized sand bath.   In  the  case  of  galvanometric  instruments
             This consists of an open vessel fitted with a porous   inaccuracies occur if sufficient care has not been
             bottom (usually made  of  sintered metal). Heated   taken in the winding of the make-up resistor or if
             air is forced up through the bottom. The vessel is   the thermocouple has been changed and the new
             filled with carefully graded sand. With the air com-   external circuit  resistance not  checked. Careless
             ing up through it the sand behaves like a liquid. it   location or make-up of the ballast resistor so that
             takes up the temperature of the air. The sand is a   one of the cold junction  terminals is too remote
             good heat transfer medium. The apparatus makes a   from  the  cold  junction  compensating  element
             most  convenient way  of  calibrating  temperature   causes  variable  errors  of  several degrees as  the
             probes. Where maximum accuracy is essential the   ambient temperature changes. Where the ballast
             thermocouple should be calibrated against one of   resistor required is of a low value, 10 ohms or so,
             the IPTS-68 secondary reference points. Table 14.5   the best arrangement may well be to use a coil of
             shows some of the points.                compensating cable of the right resistance.
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