Page 8 - Vogel's TEXTBOOK OF QUANTITATIVE CHEMICAL ANALYSIS
P. 8
CONTENTS
7.7 Liquid ion exchangers 204
APPLICATIONS IN ANALYTICAL CHEMISTRY 205
7.8 Experimental techniques 205
7.9 Determination of the capacity of an ion exchange resin (column
method) 207
7.10 Separation of zinc and magnesium on an anion exchanger 208
7.11 Separation of chloride and bromide on an anion exchanger 209
7.12 Determination of the total cation concentration in water 210
7.13 Separation of cadmium and zinc on an anion exchanger 210
7.14 Concentration of copper(I1) ions from a brine solution using a
chelating ion exchange resin 212
7.15 Determination of anions using ion chromatography 213
CHAPTER 8 COLUMN AND THIN-LAYER LlQUlD
CHROMATOGRAPHY
8.1 Introduction 216
8.2 Types of liquid chromatography 216
8.3 Equipment for HPLC 220
8.4 Derivatisation 228
8.5 Quantitative analysis 229
8.6 Thin-layer chromatography 229
8.7 High performance thin-layer chromatography (HPTLC) 232
8.8 Determination of aspirin, phenacetin and caffeine in a mixture 233
8.9 Thin-layer chromatography - The recovery of separated
substances by elution techniques 233
CHAPTER 9 CAS CHROMATOGRAPHY
9.1 Introduction 235
9.2 Apparatus 235
9.3 Programmed-temperature gas chromatography 244
9.4 Quantitative analysis by GLC 245
9.5 Elemental analysis using gas chromatography 247
9.6 Determination of aluminium by gas chromatographic analysis of
its tris(acety1acetonato) complex 248
9.7 Analysis of a mixture using the interna1 normalisation
method 249
9.8 Determination of sucrose as its trimethylsilyl derivative using
gas-liquid chromatography 250
9.9 References for Part C 251
9.10 Selected bibliography for Part C 253
