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334  Dust Explosions in the Process Industries


             4.4.3.2
             Experimental  Investigations


             The data from Eckhoff (1977), given in Figure 4.41, illustrate the influence of the igni-
             tion delay on the explosion development in a cloud of lycopodium in air in a 1.2 liter
             Hartmann bomb. As can be seen, there is little differencebetween the maximum explo-
             sion pressure obtained with a delay of 40 ms and 200 ms, whereas the maximum rate
             of pressure rise is drastically reduced, from 430 bar/s to 50 barh, that is, by a factor of
             almost 10.There is little doubt that this is due to the reduced initialturbulence in the dust
             cloud at the large ignition delays.With ignition delay increasingbeyond 200 ms, the max-
             imum explosion pressure is also reduced as the dust starts to settle out of suspensionbefore
             the ignition source is activated.

















                a   im   200   3w   400   500   600   7m   BOO   9~   IOW ms  ~1m
                                    triggering
                                         dispersion
                                             air
                               time offer triggering dispersion air  volvevolve
                               time
                                 offer
             Figure 4.41  Influence of ignition delay on development of lycopodium/air explosion in a  1.2 liter
             Hartmann’s bomb. The ignition source is a 4 J  electric spark ofdischarge time 2-3  ms. Dust concen-
             tration is 420 g/m3.Initial pressure in 60 cm3dispersion air reservoir is 8 bar(g) (FromEckhof6  1977).
               As would be expected,the same kind of influence of ignition delay as shown in Figure
             4.41 is found in all experiments of  the type illustrated in Figure 4.39. One of  the first
             researchers to observe this effect was Bartknecht (1971). Some of his results for a 1 m3
             explosion vessel are given in Figure 4.42. As the ignition delay is increased from the
             lowest value of about 0.3 s to about 1s, there is marked decrease of (dpldt),,,   whereas
             P,,,   is comparatively independent of the ignitiondelay for both dusts. If the ignition delay
             is increased further, however, there is a marked decrease even in P,,   for the coal. The
              1m3 apparatus used by Bartknecht in 1971 is in fact the prototype of the standard test
             apparatus specified by the International Standards Organization (1985).
               In this standard, an ignition delay of 0.6 s is prescribed. As Figure 4.42 shows, this is
             not the worst case, because a significantlyhigher level of initial turbulence and resulting
             rates of pressure rise exist at shorter ignition delays, down to 0.3 s. The delay of 0.6 s
             was chosen as a standardbecause, at approximatelythis moment, the dust dispersion was
             completed;that is, the pressure equilibriumbetween VI and V, in Figure 4.39 was estab-
             lished. In view of this, there is no logical argument for claiming that an ignition delay
              of 0.6 s corresponds to the “worst case.” One can easily envisage situations in industry
             where dust injection into the explosion space is continued after ignition.
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