Page 64 - Engineered Interfaces in Fiber Reinforced Composites
P. 64

Chapter  3.  Measurements  of  interfacelinterlaminar properties   47





                      HI‘/                   by = 92.6MPa

                                             End of fragmentation







                                                        Acoustic
                                                     emission events
                                I              1  ,  I
                      (b)            75 fiber ruptures

          Fig. 3.3. (a) Typical load4isplacement curve and (b) acoustic emission events for a fiber fragmentation
                test on an AS4 carbon fiber-PEEK  matrix composite. After Vautey and Favre (1990).



            The average value of fiber fragment lengths obtained at the end of the test when
          the application of stress does not cause any further fiber fragmentation is referred to
          as the  ‘critical  transfer  length’,  (2L),. The  critical  transfer  length  represents  the
          complex tensile fracture characteristics of brittle fibers and the statistical distribu-
          tion of fiber fragment lengths. Typical plots of the mean fragment length versus fiber
          stress are shown in Fig 3.4 for carbon fiber-epoxy and Kevlar 49-epoxy systems. It
          is  interesting  to  note  that  the  idea  of  the  critical  transfer  length  was  originally
          derived from the concept of maximum embedded fiber length, Lmax, above which the
          fiber breaks  without  being completely  pulled  out in  the fiber pull-out  test,  rather
          than in the fiber fragmentation test. In an earlier paper by Kelly and Tyson (1965),
           (2L), for the composite with a frictionally  bonded interface is defined as twice the
          longest  embedded  fiber  length  that  can  be  pulled  out  without  fracture,  i.e.
           (2L), = 2Lm,,.  The solution of L,,,   as a function of the characteristic fiber stresses
          and  the  properties  of  composite  constituents  and  its  practical  implications  are
          discussed in Chapter 4.
             For  analytical purposes,  the  critical  transfer  length  is  also defined as the  fiber
          length necessary to build up a maximum stress (or strain) equivalent to 97% of that
          for an infinitely long fiber (Whitney and Drzal 1987). In this case, the knowledge of
          the critical transfer  length is related  principally to the efficient reinforcement  effect
          by the fiber. (Compare this value with 90% of that for an infinitely long fiber for the
          definition of “ineffective length” (Rosen,  1964; Zweben,  1968; Leng and Courtney,
           1990; Beltzer et al.,  1992).)
            The average shear strength at the interface, z,,   whether  bonded, debonded  or if
          the  surrounding  matrix  material  is  yielded,  whichever  occurs  first,  can  be
          approximately  estimated  from  a  simple  force  balance  equation  for  a  constant
          interface shear stress (Kelly and Tyson,  1965):
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