Page 447 - Failure Analysis Case Studies II
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                                   Fig. 5. Schematic illustration of the shaft fracture surface.



            3.  Destructive examination of the shaft

            3.1. Fractography

              Figures 5 and 6 show the results obtained in the fractographic examination performed by SEM.
            The schematic illustration  of  Fig.  5  represents the different zones with  different fractographic
            characteristics.
              In the outer part, zone A (Fig. 6a), which is approximately 10 mm wide, the fracture morphology
            is mainly intergranular, with grains up to 600 pm in diameter, but showing also some small areas
            with transgranular  fracture. This morphology is constant in all the zone A, but  the grain size
            decreases considerably from the external diameter towards zone B. In zone B (Fig. 6b), approxi-
            mately 15 mm wide, progressively from zones A to C, the grain size decreases and the proportion
            of transgranular fracture increases. Close to zone C the fracture is almost transgranular, although
            some grain boundaries are still visible. Zone C (Fig. 6c), of - 5 mm width, shows a dark coloration
            due to the presence of deposits. Under the deposits there are mainly transgranular areas but also
            some intergranular facets. Grains -20  pm in diameter can be measured in this zone. Finally, the
            morphology of zone D (Fig. 6d) is typical of fatigue and torsion processes.

            3.2. Metallography of the fractured area

              Several axial metallographic sections cut from zones close to the fracture surface were prepared
            with two aims: to know if  the material was damaged in these areas, and to study their micro-
            structural characteristics, mainly grain size.
              Two different metallographic sections can be seen in Figs 7 and 8. Figure 7 shows a macro-
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