Page 232 - Fiber Fracture
P. 232

STRENGTH AND FRACTURE OF METALLIC FILAMENTS                          217

                      500
                                                    Cu wire  0 30 pm R = 0

                   -
                    7 400
                   E                   I           I  -   \-    I
                      300
                    w
                    v1
                   3
                    ;
                      200
                   .C( ?i
                    x
                   5 100



                        0
                          1          1 o2         104          106          1 os
                                       Number of cycles to rupture   d
                        Fix. 31. Fatigue curves of a 30 pm diameter Cu wirc in 3 annealing states.


             Table 5. Grain size, annealing conditions and tensile strength of Cu wires (99.97% punty) used to  measure
             the S-N  curves given in Figs. 31  and 32
             Diameter   Annealing conditions   Grain size   Yield stress, R0.2   Tensile strength
             (w)                           (elm)          (MPa)           (MPa)
             95         as drawn           <I             437             475
             30         as drawn           <I             484             514
             9.5        3 h/2.50°C         3. I           305             3.55
             30         3 h/2500C          2.5            254             302
             95         2 h/600'C          95 (bamboo str.)   70          23 1
             30         2 h/600"C          30 (bamboo str.)   81          222



               These results point out that Cu wires in the as-drawn state are superior to the same
             wires in the annealed states. This result is even more astonishing when we keep in mind
             that these wires have already been subjected to a severe low cycle 'fatigue treatment'
             when  they  were  drawn.  Strong differences become also apparent when  we compare
             curves for the two diameters in the same state. Thin wires in  the as-drawn state and
             those  with  a  bamboo structure live longer than  the  thick ones. For the  intermediate
             state the  difference is  very  small but  compared to  the  as-drawn  wires  they  show  a
             good or even better performance in  the high-cycle domain. The differences between
             the two as-drawn states are difficult to comment. These samples have very small grains
             compared to their diameter, and  the proximity of  the surface should not  affect their
             fatigue life. Figs. 33 and 34  show the fracture surface of  the as-drawn and annealed
             wires. Thin as-drawn wires (Fig. 33 left) neck down to a cone whereas in  the thicker
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