Page 106 - Book Hosokawa Nanoparticle Technology Handbook
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FUNDAMENTALS                                            CH. 2 STRUCTURAL CONTROL OF NANOPARTICLES

                                                                   270                           Spot 1
                                                                   240     SiKa
                                                                            Si
                                                                   210
                                                                   180   OKa
                    Intensity                                     Counts  150  CKa
                                                                   120
                                                                    90
                                                                    60     ZrLa     CuKa  CuKb   ZrKa  ZrKb
                                                                    30
                                                                     0
                    5      21      37     53     69      85           0.00  3.00  6.00  9.00 12.00 15.00 18.00 21.00
                                 Diffraction Angle (2θ°)
                                                                                    Energy keV
                  Figure 2.4.6                                     150
                  X-ray diffraction pattern of (La Sr 1 x )MnO  3  135     ZrLa  Zr              Spot 2
                                         x
                  nanoparticles.                                   120
                                                                   105  CKa  SiKa
                                                                  Counts  90  OKa               Zr
                                                                    75
                                                                    60
                                                                    45               CuKa  CuKb
                                                                    15                             Zr
                                                                    30
                                                                     0
                                                 1                    0.00  3.00  6.00  9.00 12.00 15.00 18.00 21.00
                                                                                    Energy keV

                                                                 Figure 2.4.8
                                                                 Analytical EDX of 50% ZrO -50% SiO nanoparticle.
                                                                                     2
                                                                                             2
                                       2






                                                                                                 v









                                                   10nm
                                                                                                  u
                  Figure 2.4.7
                  50% ZrO -50% SiO nanoparticles.
                         2      2

                                                                                                   10nm
                  independent oxides by additive and doping, materials
                  with new characteristics can be generated. The materi-
                  als for making sensors and catalysts with superior  Figure 2.4.9
                  characteristics and mechanical property are created  Al, Ca, Si, Ti, and Zr oxide nanoparticles.

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