Page 121 - Book Hosokawa Nanoparticle Technology Handbook
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2.5 PORE STRUCTURE                                                           FUNDAMENTALS


                            (a)                      (b)                     (c)









                                             X                        X                        X


                                       (d)                       (e)







                                                                                        x=100nm
                                                         X                         X


                  Figure 2.5.3
                  SEM images of porous particles prepared by spray-pyrolysis method. (a) SiO , (b) TiO , (c) ZrO , (d) Al O , (e) Y O .
                                                                                                      3
                                                                                        2
                                                                                              2
                                                                                                     2
                                                                          2
                                                                                 2
                                                                                               3
                                High concentration of sol solution
                                     Small droplet size
                                 Very large silica particles size


                                                                                          3 μm

                                                                            Solid spherical particle



                               Primary droplet







                                                 High carrier gas flow rate
                                                 Large droplet size
                                                 High temperature
                                                 Addition of surfactant                   3 μm

                                                                            Doughnut-type particle
                  Figure 2.5.4
                  Spherical and doughnut-type SiO particles prepared by spray-drying method.
                                          2
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