Page 106 - Packed bed columns for absorption, desorption, rectification and direct heat transfer
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                                  1. The absence of preliminary humidifying practically does not
                          influence the absorption and desorption processes at room temperature.
                                 2. Because the humidifying is a very rapid process, the air is humidified
                          in the space under the packing and in the first half meter of the packing height.
                                  3. The preliminary humidifying of the air with pure water leads to
                          reduction of the solution concentration in the experimental column because of
                          water vapour absorption. That is why the preliminary humidifying can be not
                          only without avail, but in some cases even harmful.
                                  4. In the industrial columns, for the calculation of which the
                          experimental data are intended, preliminary humidifying of the gas phase is not
                          provided.

                          2,1.1.3. Construction of the experimental column
                                  The experimental installations are two types, pilot plant installations
                          built to proof the apparatus suitability for a given industrial process, and
                           installations developed to obtain experimental data for the performance
                           characteristics of the packings. The date obtained in the latter type of
                           installations are used directly to design industrial columns, or to obtain
                           equations necessary for their designing. In this chapter only the second type of
                           installations is considered. They are proper for investigation of the following
                           performance characteristics of the packings:
                           - pressure drop;
                           - loading and flooding point;
                           - liquid holdup;
                           - effective surface area;
                           - gas- and liquid-side controlled mass transfer coefficient.
                                  There are some important differences in the requirements to the
                           industrial and the experimental installations. The industrial columns are
                           designed to achieve, as cheap as possible, some important technological and
                           economical parameters, i.e. to take part in lower-cost production of high quality
                           products keeping ecological conformity. The experimental installation is
                           designed to obtain, as precisely as possible, the necessary data for calculation of
                           industrial columns.
                                  The most important characteristics of the experimental installations are
                           column diameter, packing height, and liquid phase distributor construction.
                                  To avoid the influence of the ratio of the column diameter to the
                           packing diameter, respectively its characteristic dimension, on the obtained
                           data, this ratio should not be lower than 8 [1]. The height of the packing should
                           be determined in every case, so that the accuracy of the results is the highest
                                  The determination of the effective surface area and the mass transfer
                           coefficient is connected with chemical analysis of the initial and end
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