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0066_Frame_C19  Page 87  Wednesday, January 9, 2002  5:27 PM










                                                              Ti:Saph Laser 76 MHz   τ  = 200 fs
                                Solid State Diode Pumped Laser            p
                                     λ = 532 nm         ~9W         λ = 720 nm—880 nm  (1.4 eV - 1.7 eV)
                                                                      Probe Beam 5%
                               Delay ~ 1500  ps                              Beam Splitter
                                                                λ Plate
                                                                 / 2
                                                           Sample               20:1
                                                                                       Pump
                                         Dove Prism   Lens                             Beam 95%
                                                                          1 µs
                                                            60
                                         Detector
                                                Polarizer
                                                              Variable        Acousto-Optic
                                                              ND Filter
                                                                              Modulator @ 1 MHz




                               Lock-in Amplifier 1 MHz



                       FIGURE 19.60  Experimental setup of the transient thermoreflectance technique.

                       the beam on and off at a frequency of 1 MHz, resulting in thermomodulation. The probe beam passes
                       through a dovetail prism mounted on a movable stage, which is used to increase the optical path length
                       of the probe beam and hence the time delay between the pump and probe pulses. The reflection of the probe
                       beam, which is centered in the heated area, is monitored by a photodiode and sent to a lock-in amplifier set
                       to the thermomodulation frequency of 1 MHz. This yields the temporal relaxation profile of the sample.
                         Employing the TTR method as a temperature probe involves relating the measured reflectivity changes
                       to temperature changes using the material’s complex index of refraction. In most metals and dielectrics,
                       the complex index of refraction depends weakly on temperature (Price, 1947). In wavelength ranges
                       where the reflection coefficient is large, the reflectivity can be described by the linear sum of a large static
                       contribution and a small temperature-dependent modulated contribution. The corresponding change in
                                    −5
                       reflectivity is ∼10 /K. The lock-in detection at 1 MHz enables resolution of the small transient signal.
                       By comparing the transient thermal response of a surface to the appropriate heat conduction model,
                       thermophysical properties such as the thermal diffusivity and the thermal boundary resistance can be
                       measured (Hostetler et al., 1997; Hostetler et al., 1998; Smith et al., 2000).

                       Closing Comments
                       A wide variety of sensors are available for monitoring the parameter we refer to as temperature. The choice
                       of the appropriate sensor is highly dependent upon the actual physical configuration of the measured
                       material, as well as the required precision, accuracy, and display or processing of the temperature. While
                       thermocouples may be an excellent choice for situations involving electrical logging of a remote process,
                       a gas-bulb thermometer may be adequate and more appropriate for monitoring remote temperatures
                       divorced from electricity. The physical geometry, which often limits access to the area of interest, is another
                       important consideration. It is also important to consider the accuracy requirement, as well as the spatial
                       and temporal resolution desired. This discussion is meant to provide a cursory overview of a wide array
                       of temperature-sensing techniques. There are many excellent, comprehensive references and the designer
                       is referred to these for more details. Temperature measurement often resembles an art rather than a
                       science, with new and creative techniques for monitoring thermal responses in continuous development.



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