Page 353 - Applied Process Design For Chemical And Petrochemical Plants Volume II
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342                       Applied Process Design for Chemical and Petrochemical Plants

           (text continuedhtn page 339)                          system in question by the packing manufacturer, referenc-
                                                                 ing to a specific packing size and style. Several competitive
               vapor capacity factor that in the vacuum systems is less   designs are often helpful for a final design selection.
               than 60%-70% of the corresponding flood point (the
               actual decrease depending on the mixture). The aver-   The test studies of several different structured packings
               age optimum load factor is given [123]:           of Dean et al. [ 1171 indicated that structured packing per-
                                                                 forms well in water removed by  triethylene glycol (TEG)
                                                        (9 - 78)   from natural gas from field wells, giving a design point of
                                                                 F,  = 3 (where F,  = V, I&, V,  = superficial velocity, pg = gas
             2. Specific efficiency of packing:                  density) for sizing. A high efficiency drip-point distributor

               n,/H  = 5, theoretical trays/meter                is recommended, because it was far superior to a notched
                                                                 trough or spray nozzle distributor. Excellent turndown to
             3. Average pressure drop per theoretical tray:      12:l was shown, still meeting outlet gas low water vapor
                (Ap/nJOpt  = 5 mm water column                   specifications. HETP values ranged from 44 in. to 102 in.,
                                                                 in this application. The number of theoretical trays was 2.8
               where  H = height of packing, m                   to  4.6,  varying with  liquid  and  gas  rates  and  packing
                     n, = number of theoretical trays
                     Ap  = pressure drop, mm water column        style/size. Flooding occurred at 2.28 to 3.98 F, value at 0.7
                     u,, = vapor velocity per unit of free column cross-   gpm/ft2 at 650 psig.
                         section, m/sec                            A  commercial  4ft  diameter  refinery  depropanizer
                     pv = density of vapor, kg/m3                unit’s performance after replacement of the lower half of
                                                                 a trayed tower with Intalox-2T (R) structured packing is
           Guidelines for Structured Packings
                                                                 described in Reference 118.
             1. Pressure drop: Range usually 0.3-0.5  in. water/ft,  or,   Nutter  [141]  Montz  B-1  structured  packing, licensed
               30-40  mm water/m of packed height [ 1161.        from Julius  Montz  GmbH of  Hilden, Germany, Figures
             2. Lower  holdup  of  liquid:  Less  than  other packings,   9-6LL and 9-6MM, is of uniform sinusoidal corrugations,
               may require special attention to operational controls.   which avoids sharp corners. The embossing on both sides
             3. More difficult to purge: Operating vapors more diffi-   of  the sheet metal is closely spaced projections in a dot-
               cult to purge from the system than random packings   matrix pattern, which spreads the liquid in a uniform film
               and trays.  This poses  potential fire, explosion, and   [141], without holes or slots. The  design  allows for  an
               toxic hazard.                                     effective liquid-vapor seal at the tower wall by means of a
             4. Lower pressure drop for vacuum systems: Allows for   metal wiper band. A representative performance is shown
               better low pressure and vacuum system operation and   for pressure  drop, Figure  9-66, and HETP, Figure 9-67.
               lower bottoms temperature, with less degradation of   This packing is effectively used in low pressure  (or vacu-
               bottoms product.                                  um) columns where large theoretical stages and low pres
             5. Internal  uniform  distribution:  Properly  designed   sure  drop  are  required,  producing  the  lowest  possible
                devices to distribute and redistribute liquid entering   pressure drop per stage. Style El is embossed sheet metal;
                the column is critical to obtain best performance of   Style BSH,  is expanded textured sheet metal, high  effi-
                these types of packings.                          ciency with maximum surface area; and Style A-3 is wire
             6. Material of construction: The materials of fabrication   gauze construction.
                For  this type of packing are more critical to long life
                due to pad size, wall thickness of metal or plastic com-
                ponents, and  actual selection based  on  the  system   Structured Packing Scale-up
                corrosion, hydrogen attack, and oxygen attack in the
                column environment.                                Applications of structured packing into ethylene plant’s
             7. HETP  values:  Small packing with  narrow corruga-   various  column  systems  [ 1191  have  been  successfully
                tions gives low HETP values, but usually higher pres-   achieved, but the individual manufacturers must be con-
                sure drops. Plastic and some metal packing sheets,   sulted to use their most directly applicable pilot and com-
                wires  or  corrugations  may  require  special surface   mercial data, which are generally not published. The use
                treatment to ensure good wettability.             of published general correlations should only be used for
              8. Preliminary designs: These can usually be made from   a  “first” or approximation design, while  the  delicate or
                the generalized literature references; however, they   important final design must be performed in cooperation
                are not a substitute for direct design of  the specific   with the manufacturer.
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