Page 306 - Chemical Process Equipment - Selection and Design
P. 306

270  DRYERS AND  COOLING  TOWERS
                         TABLE 9.14.  Performance Data of Fluidized Bed Dryers: Batch and Multistage Equipment
                         (a)  Batch Dryers

                                                                   Lactose
                                                       Ammonium     Base    Pharmaceutical   Liver   Weed
                                                        Bromide   Granules     Crystals   Residue   Killer
                         Holding capacity (Ib wet product)   100    104         160         280     250
                         Bulk density, dry (lb/ft3)       75         30          20         30      35
                         Initial moisture (% w/w basis)    6         10          65         50     20-25
                         Final moisture (% w/w basis)      1         2           0.4        5.0     1 .o
                         Final drying temperature (“F)    21 2      158         248         140     140
                         Drying time (min)                20         90         120         75      21 0
                         Fan capacity (ft3/min at 11 in. w.g.)   750   1500     3000       4000     3000
                         Fan HP                            5         10          20         25      20
                         Evaporation rate (Ib H,O/hr)     15         5.7         52         100     17
                            (Courtesy Calmic Engineering Co. Ltd.; Williams-Gardner,  1971 1.

                          (b) Multistage Dryers with Dual-flow Distributors [Equipment Sketch in Fig. 9.13(b)]

                                           Function                  Heater    Cooler     Drier    Cooler
                                                                     Wheat     Wheat               Quartz
                                           Material                  Grains    Grains     Slag     Sand

                          Particle size (diameter)(mm)                5x3       5x3        0.95      1.4
                          Material feed rate (metric tons/hr)          1.5       1.5       7.0       4.0
                          Column diameter (m)                          0.90      0.83      1.60      1.70
                          Perforated trays (shelves):
                           Hole diameter (mm)                          20       20       20;  10    20
                           Proportion of active section                0.4       0.4     0.4;  0.4   0.4
                           Number of trays                            10         6        1;  2     20
                           Distance between trays (mm)                20        20       25;  40    15
                          Total pressure drop on fluidized bed (kgf/mz)   113   64        70 a      40
                          Hydraulic resistance of material on one tray (kgf/m2)   7.8   9.2   20;  10   1.8
                          Inlet gas temperature (“C)                 265        38       300        20
                          Gas inlet velocity (m/sec)                   8.02      3.22      4.60      0.74
                          Material inlet temperature  (“C)            68       175        20       350
                          Material discharge temperature (“C)         175       54       170        22
                          Initial humidity (% on wet material)        25         -         8        -
                          Final humidity (% on wet material)           2.8       -         0.5      -
                          Blower conditions
                           Pressure (kgf/m*)                         450       250       420       250
                           Throughput (m3/min)                        180      130       360       100
                                                                      (80°C)    (50°C)   (70°C)    (35°C)
                           Power consumption (HP)                     50        20        75         7.5
                             a With grids and two distributor plates.
                             (Romankov, in Davidson and Harrison, Fluidisation, Academic,  New York,  1971).

                drying time is a particular advantage with  heat  sensitive materials.   Residence times of  air  and particles are  far from uniform; Figure
                Porosity  and  small  size  are  desirable  when  the  material  sub-   9.5(a) and (b) is a sample of  such data.
                sequently is  to be  dissolved (as  foods or  detergents)  or dispersed   Because of  slip and turbulence, the average residence times of
                (as  pigments,  inks,  etc.).  Table  9.17  has  some  data  on  size   particles are  substantially greater  than  the  mean  time  of  the  air,
                distributions, bulk  density, and power requirements of  the  several   definitely so  in the  case of countercurrent  or mixed  flow.  Surface
                types of  atomizers.                                moisture is removed rapidly, in less than 5 sec as a rule, but falling
                   The mean residence time of  the gas in a spray dryer is the ratio   rate  drying  takes  much  longer.  Nevertheless,  the  usual  drying
                of  vessel volume to the volumetric flow rate. These statements are   operation is completed in 5-30 sec. The residence time distribution
                made in the literature regarding residence times for spray drying:   of  particles is  dependent  on  the  mixing behavior  and  on the  size
                                                                    distribution.  The  coarsest  particles  fall  most  rapidly  and  take
                                                                    longest for  complete drying. If  the material is heat-sensitive, very
                               Source              Time (sec)
                                                                    tall  towers  in  parallel  flow  must  be  employed;  otherwise,
                   Heat Exchanger Design Handbook (1983)   5-60     countercurrent  or  mixed  flows  with  high  air  temperatures  may
                   McCormick (1979)              20                 suffice. In  some cases it  may be  feasible to  follow up  incomplete
                   Masters (1976)                20-40  (parallel flow)   spray drying with a pneumatic dryer.
                   Nonhebel and Moss (1971)      160                   Drying  must  be  essentially  completed  in  the  straight  sided
                   Peck (1983)                   5-30
                   Wentz and Thygeson (1979)                        zones of  Figures 9.14(a) and (b). The conical section is for gather-
                   Williams-Gardner  (1971 )     4-10  (<15ftdia)   ing and efficient discharge of the  dried product.  The lateral throw
                                                 10-20  (>15ftdia)   of  spray  wheels  requires  a  vessel  of  large  diameter  to  avoid
   301   302   303   304   305   306   307   308   309   310   311