Page 284 - Academic Press Encyclopedia of Physical Science and Technology 3rd Chemical Engineering
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 Encyclopedia of Physical Science and Technology  EN006C-252  June 27, 2001  14:15







               84                                                                                       Fluid Mixing


               are used more often than not. Wall baffles for low-viscosity  TABLE I  Elements of Mixer Design
               systems consist of four baffles, each   1  of the tank diam-
                                             12                            Process design
               eter in width. Another method is to install an axial flow      Fluid mechanics of impellers
               impeller type in an angualar, off-center position, such that  Fluid regime required by process
               it  gives  good  top-to-bottom  turnover,  avoids  vortexing,  Scaleup; hydraulic similarity
               and also avoids the use of baffles. Figure 11a shows a typ-  Impeller power characteristics
               ical flow pattern for an unbaffled tank. A baffled tank axial    Relate impeller hp, speed, and diameter
               radial flow is shown in Fig. 11b, and the angular off-center  Mechanical design
               position is in Fig. 11c.                                      Impellers
                                                                             Shafts
                                                                             Drive assembly



                                                                   The need to use wall baffles to eliminate vortexing de-
                                                                 creases as fluids become more viscous (5000–10,000 cP
                                                                 or more). But swirl will still be present if there are no
                                                                 baffles. Accordingly, quite often baffles of about one-half
                                                                 normal width are used in viscous materials. In such cases
                                                                 they are placed about halfway between the impeller and
                                                                 the wall.


                                                                 C.  Power Consumption
                                                                 Table I shows the three areas of consideration in mixer
                                                                 design.  The  first  area  is  process  design,  which  will  be
                                                                 covered in detail in succeeding pages. Process design en-
                                                                 tails determining the power and diameter of the impeller
                                                                 to achieve a satisfactory result. The speed is then calcu-
                                                                 lated by referring to the Reynolds number–power number
                                                                 curve, shown in Fig. 12. Such a curve allows trial-and-
                                                                 error calculations of the speed once the fluid properties,
                                                                  P, D, and the impeller design are known.


                                                                 D. Process Considerations
                                                                 Table II gives a representation of the various types of mix-
                                                                 ing processes. The second column lists the nine basic areas
                                                                 of mixing: gas-liquid, liquid-solid, liquid-liquid, miscible
                                                                 liquid, fluid motion, and combinations of those. However,
                                                                 of more importance are the two adjacent columns. The
                                                                 first column includes physical processing, and has mixing
                                                                 criteria which indicate a certain degree of uniformity. The
                                                                 thirdcolumnhaschemicalandmasstransferrequirements,
                                                                 which involve the concept of turbulence, mass transfer,
                                                                 chemical reactions, and microscale mixing. Thus, there
                                                                 are summarized ten separate mixing technologies, each
                                                                 having its own application principles, scaleup rules, and
                                                                 general effect of process design considerations. In a com-
               FIGURE 11  Effect of baffles in position on flow pattern. (a) Typi-  plex process such as polymerization, there may possibly
               cal swirling and vortexing flow in a tank without baffles. (b) Typical  exist solids suspension, liquid–liquid dispersion, chemi-
               top-to-bottom flow pattern with radial flow impellers with four wall
               baffles. (c) Typical angular off-center position for axial flow im-  cal reaction, blending, heat transfer, and other important
               pellers to give top-to-bottom flow pattern to avoid swirl without the  steps. In general, it is more advantageous to break the pro-
               use of wall baffles.                               cess down into the component steps and consider the effect
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