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56                Engineered interfaces in fiber reinforced  composites






















                               0.1 :        1        I         I        I
                                  0       200       400      600      800      11
                                         Approximate droplet size (pm)

                    Fig. 3.10. Effect of curing cycle on the fraction of amine curing agent estimated to have diffused out of
                                   droplets as a function  of their size. After  Rao et al. (1991).

                    this test, a central fiber is pulled out of a seven-fiber microcomposite as shown in Fig
                    3.11. Great difficulties are encountered in constructing the specimens since accurate
                    control of the geometry determines the embedded fiber length. No clear correlations
                    exist between the IFSS and the fiber volume fraction. This indicates that the actual
                    failure mechanisms during fiber pull-out  are matrix dominated (Qiu and Schwartz,
                    1993).

                    3.2.5.  Microindentation  (or jiber push-out)  test

                      The microindentation technique (or ‘push-out’ test as opposed to the ‘pull-out’ test)
                    is a single fiber test capable of examining fibers embedded in the actual composite. The

                                  Surrounding fiber (six)        Centy fiber








                                                  /            \

                                        PET fiber knot         Epoxy bonded part

                                Fig. 3.1 1. Schematic presentation of a multi-fiber pull-out  specimen
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