Page 106 - Failure Analysis Case Studies II
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                                                  HOT BLADE
        Fig. 9. Weld formation in final closure of plastic panels to form large diameter hoop. The panels are bent round to meet
        a hot knife, the knife is withdrawn, and the two ends pressed together to form the final joint. One problem is that the
        panels are still in a state of strain, which is not relieved. Stress relaxation will occur with time, but residual stresses may
        contribute to early failures if the design itself is faulty.



        present, the spark would travel through the gap and the defect be discovered. The method was
        relatively crude, and could not detect pinholes which did not connect the two opposite surfaces of
        the weld, for example.
          The large circumferential hoops are created first, in the following way. Flat sheets previously
        cut to the appropriate length with the table saw are welded up until the last joint is ready to be
        made. The ca 8.55 m length (in the case of the failed tank) is then bent round by hand to form a
        complete circle, and the ends thermally welded by  the machine to make the hoop (Fig. 9). The
        hoop is therefore under a continuous bending stress, with a large tensile component in the outer
        surface, and a compressive component on the inner. This is discussed further, especially the effect
        on the gross stress to which the welds are exposed as a result, in Part I1 of this investigation.
          Similar hoops made in the same way  are then stacked and welded  to create the tower.  The
        operator thought that the horizontal welds thus made were somewhat weaker than the butt welds
        made initially, but certainly much stronger than hand made welds.



        7.  Materials analysis programme

          Material from both panels and welds was also tested for its chemical integrity. The tests employed
        included infra-red spectroscopy (using a Fourier Transform or FTIR spectrometer) and melting
        behaviour (using a Differential Scanning Calorimeter or DSC). The objective in these tests was to
        see if there were any perceptible differences in chemical behaviour between ‘good’ and ‘poor’ weld
        material, between weld  and panel material and between independent samples of polypropylene
        and material taken from the tank.
          FTIR spectroscopy showed that the tank material was an ethylene-propylene copolymer. Little
        variation in chemical composition could be detected from several weld sample and normal tank
        material. Moreover, there was no evidence of  oxidation, especially in the welds. The results of
        various DSC experiments conducted on the various tank materials are shown in Table 2.
          The thermograms showed that both sets of samples had very similar endotherms, with melting
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