Page 157 - Failure Analysis Case Studies II
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          the grains and at grain boundaries (Fig. 4). Hairline cracks were clearly visible along some of the
          grain boundaries.
            The surface of the weld showed a nitrided layer which was cracked at regular intervals (Fig. 5).
          Sections of the surface adjacent to the weld bead clearly showed the white layer from the nitriding
          process. Surface cracks were visible. Since the white layer was not present in the crack (Fig. 6), these
          cracks probably originated after the nitriding process.
            Some of  the areas on the adapter that were supposed to have been blanked  by  the refractory
          compound were carburised. This showed that the blanking procedure was not adequate and resulted
          in the low weldability of the adapter.
            The fracture  surfaces showed no  signs of  fatigue.  Fracture  was intergranular  and numerous
          intergranular cracks were visible on the fracture surfaces (Fig. 7).




























           Fig. 4. Optical micrograph of one of the E312 welds showing severe carbide precipitation (etchant: Beraha's tint etch).




























            Fig. 5. Optical micrograph of the E312 weld showing cracks that originated after the nitriding (etchant: 2% Nital)
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