Page 93 - Handbook of Materials Failure Analysis
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2 Case History     87




                                                    Catalogue data - mean curve
                      100
                                                    Catalogue data - minimum curve
                                                    Sample A - as supplied
                                                    Sample B3 (deformed) - after 114000h
                                                    Sample B1 (deformed) - after 90000h
                                                    Sample B4 (undeformed) - after 114000h

                     Stress (MPa)                                   Interrupted



                                                                      test







                       10
                         29       30       31       32      33       34       35
                                                   LMP
                  FIGURE 4.15
                  Larson miller diagram (C¼22.9): experimental creep data for samples type A (as supplied)
                  and type B after 90,000 h and 114,000 h of service. Larson-Miller curves supplied by the
                  manufacturer catalogue [21]: average values (––––) and minimum values (     ).


                     Available creep test data performed on a tube of the same plant (sample B1),
                  decommissioned after 90,000 h of service with maximum diameter deformation
                  around 1.5% are also plotted.
                     On the basis of creep test results, the following considerations can be drawn:
                  •  creep test result for type A specimen (as supplied) are consistent with the
                     manufacturer minimum creep values;
                  •  creep test results for B4-1 and B4-2 samples (taken after service from
                     undeformed sections) are very close to the “as-supplied” behavior;
                  •  the representative points of specimens (B3) and (B1), taken after service from
                     deformed sections, are well below the manufacturer creep curves, due to creep
                     damage accumulated during service;
                  •  creep test results of samples taken from deformed sections, after 114,000 h of
                     service (B3), are well aligned with creep test results obtained from similar
                     sections of tubes removed from service after 90,000 h (B1);
                  •  creep ductility is quite low for the “as-supplied” type A sample (7%), while it is
                     higher for type B3 and B1 samples (nearly 40%).
                  As described in Ref. [30], the tube residual life was estimated by means of an exper-
                  imental master curve, obtained correlating creep test results of B3 and B1 samples.
                  Therefore, assuming σ ¼17.5 MPa (hoop stress at design pressure), the LMP values
                  (Figure 4.15) and then the corresponding rupture time at different temperatures
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