Page 105 - Chalcogenide Glasses for Infrared Optics
P. 105

Glass Pr oduction    83





                    10 ×
                      3








                    10 ×                       Experimental data
                      2
                  Viscosity (p)







                    10 ×
                      1
                                                   Prior estimate
                                                   (extrapolated from 10 7.6
                                                   p & 10 4.7  p data points)






                      0
                    10 ×
                       500           600           700           800
                                       Temperature (°C)
              FIGURE 3.11  Viscosity of TI 1173 glass measured in liquid range.


              two average results were compared, the recast index increased by
              about +0.0040. The increase was thought to be due to loss of Se and
              Ge-Se vapors. The optical designer could then decide if glass could be
              recast once, twice, or even 3 times and used based on the index change
              and system design parameters such as focus. The dispersion param-
              eters for the glass were left relatively unchanged.
                 Figure 3.12 shows the final configuration of the casting furnace
              used at TI for TI 1173 glass. The chamber enclosure is round and large
              with a single door in front. Inside is a large quartz crucible that holds
              all the glass to be cast. Heaters are provided to melt and control the
              temperature of the glass. Provisions are made for a powered stirring
              device controlled from the top. A rod from the top is connected to the
              ball joint in the bottom of the crucible that allows glass to flow into
              the mold in the bottom chamber. Provisions are made for heating the
   100   101   102   103   104   105   106   107   108   109   110