Page 211 - Engineered Interfaces in Fiber Reinforced Composites
P. 211

193


                                                                -1.5%


                                                                -2.0%
                                                                -2.5%

                                                                -3.5%

                                                                -4.5%

                                                                -6.0%




              Fig. 5.16.  Photoelastic  patterns of carbon  fibers in  an epoxy  matrix  (a) without  and  (b) with  surface
              treatment,  at varying applied strains. After  Drzal et 211.  (1983a). Reproduced  by  permission  of Gordon
                                       and  Breach Science Publishers.

              This  is  attributed  to  the  load  increase  required  to  cause  the  interface  failure  in
              transverse  tension  due to  the  Poisson  effect  under  compression.  In  contrast,  the
              tensile and compressive moduli are relatively insensitive to changes in the interface
              bond strength (Fig. 5.17(b)). However, for very high bond strength, the compressive
              modulus  shows a  marginal  increase,  due presumably  to the  presence  of  a  brittle
              interphase  surrounding  the carbon fibers. There is  little  difference, within  experi-
              mental scatter, between the flexural strength and bending moduli of the composites
              with  low  and  intermediate  interface  bonding.  But  for  the  composites  with  the
              strongest  interface  bond  strength,  there  is  a  significant  increase  in  the  flexural
              strength  due to a change in  the  failure mode. That is, from  an interface-initiated
              mode to a predominantly tensile (or compressive) mode.
                The average values  of  the  off-axis properties  for  three  different  composites  are
              summarized in Table 5.7. It is noted that all strength values measured are sensitive
              to the level of interface bonding, while the modulus values are relatively insensitive
              to the interface adhesion.  In particular, the transverse tensile and flexural strengths
              are  a  good  indication  of  the  interfacial  adhesion.  In  case  of  ILSS,  the  results
              obtained  from the Iosipescu shear test  method  show the  least scatter amongst the
              three types of mechanical tests carried out. SEM study shows that the failure in both
              Iosipescu and short beam shear test specimens are matrix-dominated, while the * 45
              tension specimen is relatively insensitive to the variation of failure modes. Although
              the transverse tensile and transverse flexural modulus values are similar in terms of
              absolute  magnitude  and  insensitivity  to  the  interface  adhesion  level,  there  are
              significant  differences  between  the  transverse  tensile  and  transverse  flexural
              strengths. The transverse  flexural  strength  is  more  sensitive to interface bonding,
              and is  much  higher  than the  transverse tensile strength. This observation  may  be
              explained  in  terms  of  the  non-uniform  stress  distribution  across  the  thickness  of
              the specimen in  three-point bending.  In contrast,  in  transverse  tension,  the whole
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