Page 210 - Fluid mechanics, heat transfer, and mass transfer
P. 210

MIXING
            188
                 & There are four main types of mixing equipment,      convective and diffusive mechanisms of mixing, and
                  namely,  tumbler,  convective,  hopper,  and         gentle mixing for friable particles. This type of
                  fluidization.                                         rotating mixer comes in double cone or V-shaped
               . What  are  tumbler  mixers?  What  are  their         configurations, and in some cases, these geometries
                characteristics?                                       are given asymmetric features to reduce mix times
                 & Tumbler mixers operate by tumbling the solids inside  and improve mix uniformity.
                  a revolving vessel.                                & Operate at speeds up to about 100 rpm (about half the
                                                                       critical speed, at which the centrifugal force on the
                 & May be fitted with baffles to assist mixing or with
                                                                       particles exceeds the pull of gravity).
                  internal rotating devices to break up agglomerates.
                                                                       ➢ Rotational speed is generally not as important of a
                 & The tumbler mixer is a mainstay in the pharmaceu-
                                                                         factor in achieving uniformity as loading method
                  tical and food industries because of its features of
                                                                         and mix time, based on the number of rotations.
                  close quality control in batch operation, effective
                                                                     & Working capacity is about 50–60% of volume. Ca-
                                                                       pacities are in the range of 0.014–5.66 m 3
                                                                                3
                                                                       (0.5–200 ft ).
                                                                     & Best suited for gentle blending of particles with
                                                                       similar physical characteristics; segregation can be
                                                                       a problem.
                                                                     & Equilibrium is generally reached in about 10–15 min.
                                                                     & Typically, a top-to-bottom component loading is
                                                                       better than a side-to-side loading with tumbler
                                                                       mixers.
                                                                       ➢ With top-to-bottom loading, ingredients are al-
                                                                         lowed to cascade into one another with diffusive
                                                                         effects occurring perpendicular to the main flow.
                                                                         This approach yields far faster mixing times than
                                                                         side-to-side loading, whereby diffusive mixing
                                                                         paces, and greatly increases, the mixing time.
                                                                       ➢ It is also important to avoid ingredient adherence
                                                                         to the walls of the mixer. This is common with fine
                                                                         additives, such as pigments and fumed silica, and
                                                                         component loss can occur if the material does not
                                                                         leave the wall surface.
                                                                       ➢ In some cases, the sticky ingredient can be pre-
                                                                         mixed into another component, a practice known
                                                                         as master batching, to help predisperse the mate-
                                                                         rial and prevent wall adherence.
                                                                       ➢ Mix cohesiveness, which directly correlates to the
                                                                         tendency of a material to form a bridge over the
                                                                         outlet of the mixer, must also be considered.
                                                                       ➢ Highly cohesive blends should not be handled in
                                                                         tumbler mixers if bridging or rat holing flow
                                                                         obstructions have been experienced in past pro-
                                                                         cessing equipment.
                                                                       ➢ To reduce mixing process bottlenecks and segrega-
                                                                         tion potential, tumbling in-bin mixers have been
                                                                         developed where the storage container, called an
                                                                         intermediate bulk container, itself becomes a mixer.
                                                                       ➢ Mix components can be loaded into the container,
                                                                         mixed, and transferred in the container to the point
                                                                         of use or to a storage area.
                                      Solids mixer.
                         FIGURE 6.19
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