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                       Fracture Testing of Nonmetals                                               369


                       8.1.5 EXPERIMENTAL ESTIMATES OF TIME-DEPENDENT FRACTURE PARAMETERS

                       While J  values and J-R curves may be indicative of a polymer’s relative toughness, the existence
                             Ic
                       of a unique correlation between J and the crack-growth rate is unlikely. Parameters such as J  may
                                                                                                 v
                       be more suitable for some viscoelastic materials. For polymers that experience large-scale yielding,
                       neither J nor J  may characterize crack growth.
                                  v
                          This section outlines a few suggestions for inferring crack-tip parameters that take into account
                       the time-dependent deformation of engineering plastics. Since most of these approaches have yet
                       to be validated experimentally, much of what follows contains an element of conjecture. These
                       proposed methods, however, are certainly no worse than conventional J integral approaches, and
                       may be considerably better for many engineering plastics.
                          The viscoelastic J integral J  can be inferred by converting physical displacements to pseudo
                                                 v
                                                                                                     e
                       displacements. For a constant rate test, Equation (8.11) gives the relationship between ∆ and ∆ .
                       The viscoelastic J integral is given by Equation (8.13); J  can also be evaluated directly from the
                                                                     v
                                      e
                       area under the P-∆  curve:
                                                            η  ∆ e
                                                        J =  b ∫ 0  Pd∆ e                        (8.28)
                                                         v
                       for a specimen with unit thickness. If the load-pseudo displacement is a power law (Equation (8.18)),
                       Equation (8.28) becomes

                                                            η M()∆ eN+1
                                                        J =                                      (8.29)
                                                         v
                                                             bN + ) 1
                                                              (
                       Comparing Equation (8.29) and Equation (8.15) leads to

                                                             b   M
                                                                ∂ 
                                                       η =−                                    (8.30)
                                                            M   a  ∆
                                                                ∂  e
                       Since M does not depend on time, the dimensionless η factor is the same for both J and J .
                                                                                                v
                          Computing pseudo-elastic displacements might also remove hysteresis effects in unloading
                                                                                       e
                       compliance tests. If the unload-reload behavior is linear viscoelastic, the P-∆  unloading curves
                       would be linear, and the crack length could be correlated to the pseudo-elastic compliance.
                          Determining pseudo displacements from Equation (8.11) or the more general expression
                       (Equation (8.10)) requires a knowledge of E(t). A separate experiment to infer E(t) would not be
                       particularly difficult, but such data would not be relevant if the material experienced large-scale
                       yielding in a fracture test. An alternative approach to inferring crack-tip parameters that takes time
                       effects into account is outlined below.
                          Schapery [10] has suggested evaluating a J-like parameter from isochronous (fixed time) load-
                       displacement curves. Consider a series of fracture tests that are performed over a range of crosshead
                       rates (Figure 8.12(a)). If one selects a fixed time and determines the various combinations of load
                       and displacement that correspond to this time, the resulting locus of points forms an isochronous
                       load-displacement curve (Figure 8.12(b)). Since the viscoelastic and yield properties are time
                       dependent, the isochronous curve represents the load-displacement behavior for fixed material
                       properties, as if time stood still while the test was performed. A fixed-time J integral can be defined
                       as follows:

                                                        η   ∆   
                                                                ∆
                                                     J = b ∫  Pd                               (8.31)
                                                          
                                                      t
                                                                 
                                                            0
                                                                  t=constant
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