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354    IDT MICROSENSOR FABRICATION

   12.3.2  TMS PECVD    Process  and Conditions

  One  of  the  necessary  conditions  for  the  deposition  of  SiO 2  is  that  the  temperature  of
  deposition  should  be  as  low  as  possible.  This  is  desirable  because  higher  temperatures
  can  adversely  affect  the  poling  characteristics  of  quartz  (in  spite  of  the  fact  that quartz
  is  a  naturally piezoelectric  material)  and  because  the  melting point  of  the  metallisation
  layer (aluminum is  650 °C) should not be  exceeded.
     We  should  therefore  choose  SiO 2  that  is  either  sputtered  or  deposited  by  plasma-
  enhanced  chemical  vapour  deposition  (PECVD)  from silane gas.  The  sputtering process
  provides  better  step-coverage  than  evaporation  and  far  less  radiation  damage  than  E-
  beam evaporation (Campbell  1996). A simple sputtering system consists of a parallel-plate
  plasma reactor in a vacuum chamber and the target material (SiO 2) placed on the  electrode
  such that it receives the maximum ion flux. An inert gas (at a pressure of 0.1  torr) is usually
  used  to supply the  chamber with high-energy ions that strike the  target  at high  velocities
  and  dislodge  the  SiO 2  molecules,  which deposit  conformal to  the  wafer  (the SAW-IDT
  device).  The  only disadvantage  in  this  process  is  that  on  account of  the  physical nature
  of the process, sputtering  could  also bombard  and damage  the delicate IDT fingers on the
  surface  of  the  quartz. Sputtering can  also  introduce a  variety of  contaminants  from  the
  substrate  holder  because  of  the  physical nature of  the  process.  Hence,  sputtering is  not
  the  ideal  means  of  depositing  SiO 2,  despite  the  fact  that  the  process  can  be  carried  out
  under conditions  of  low temperature.
     An  alternative approach  is to  use  chemical  vapour deposition  (CVD). A  simple  CVD
  process  is  shown in Figure  12.5.  The  reactor  consists  of  a tube with a rectangular  cross
  section, and the walls of the tube are maintained at a temperature T w. A single wafer  rests
  on  a heated  susceptor  in the centre of  the tube.
     This  susceptor is maintained at a temperature T s (where  T s  T w). The obvious choice
  is to  use  oxidised  silane  gas  (SiH 4)  (also referred to  as tetraethoxysilane TEOS)  to  form
       in the  presence of  an oxidising  agent,  such as O2, and  an  inert carrier  gas,  such  as
  SiO 2
  H2 (to improve the uniformity  of deposition). Excessive homogeneous reactions occurring
  spontaneously in the gas above  the wafer  will result in the deposition  of large Si particles
  in  the  gas  phase,  and  their  subsequent deposition  on  the  wafer  will  cause  poor  surface
  morphology  and inconsistent  film properties.





















                    Figure  12.5  A simple CVD process flow system
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